Ионная хроматография

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Ion chromatography
Ion chromatography
4HEôIDEALôMETHODôFORôANALYZINGôANIONSôCATIONSôANDôPOLARôSUBSTANCESôISôIONôCHROMATOGRAPHYô)TôCANôBEôUSEDôTOôRELIABLYôQUANTIFYôSUBSTANCESôTHROUGHOUTôAôWIDEôCONCENTRATIONô
RANGEô!ôWHOLEôVARIETYôOFôIONSôCANôBEôANALYZEDôINôAôSINGLEôDETERMINATIONô#OMPLETEô
AUTOMATIONôOFôIONôCHROMATOGRAPHYôISôEASYôANDôHELPSôTOôSAVEôTIMEôANDôREDUCEôCOSTSô
$UEôTOôITSôRELIABILITYôANDôROBUSTNESSôIONôCHROMATOGRAPHYôISôUSEDôINôMANYôDIFFERENTô
FIELDSôOFôAPPLICATION
Contents
Professional IC Systems
850 Professional IC
Professional IC 850
introduction
IC.11
Professional IC – ProfIC Systems
How to choose the right ProfIC system
«ProfIC 1 – Cation»
Professional IC system for automated ion chromatography
«ProfIC 2 – Cation»
Professional IC system with inline ultrafiltration
Metrohm inline ultrafiltration and dialysis
«ProfIC 3 – Cation»
Professional IC system with inline dialysis
«ProfIC 4 – Cation»
Professional IC system with inline dilution
«ProfIC 5 – Cation»
Professional IC system with variable sample preconcentration
«ProfIC 6 – Cation»
Professional IC system with inline dilution and ultrafiltration
«ProfIC 7 – Cation»
Professional IC system with inline dilution and dialysis
«ProfIC 8 – Cation»
Professional IC system with inline sample preconcentration
and matrix elimination
«ProfIC 9 – Cation»
Professional IC system for trace analysis with inline calibration,
sample preconcentration and matrix elimination
«ProfIC 15 – Cation» Professional IC system for partial loop injection
«ProfIC 1 – Anion»
Professional IC system for automated ion chromatography
Reproducibility of the suppression
Sequential suppression
«ProfIC 2 – Anion»
Professional IC system with inline ultrafiltration
«ProfIC 3 – Anion»
Professional IC system with inline dialysis
«ProfIC 4 – Anion»
Professional IC system with inline dilution
«ProfIC 5 – Anion»
Professional IC system with variable sample preconcentration
«ProfIC 6 – Anion»
Professional IC system with inline dilution and ultrafiltration
«ProfIC 7 – Anion»
Professional IC system with inline dilution and dialysis
«ProfIC 8 – Anion»
Professional IC system with inline sample preconcentration
and matrix elimination
«ProfIC 9 – Anion»
Professional IC system for trace analysis with inline calibration,
sample preconcentration and matrix elimination
«ProfIC 10 – Anion»
Professional IC system with inline sample preconcentration,
matrix elimination and matrix neutralisation
«ProfIC 11 – Anion»
Professional IC system for trace analysis with inline calibration,
sample preconcentration and matrix elimination
«ProfIC 12 – Anion»
Professional IC gradient system
«ProfIC 15 – Anion»
Professional IC system for partial loop injection
«ProfIC 1 – AnCat»
Professional IC system for automated ion chromatography
«ProfIC 2 – AnCat»
Professional IC system with inline ultrafiltration
«ProfIC 15 – AnCat» Professional IC system for partial loop injection
IC.13
IC.14
IC.15
IC.16
IC.17
IC.18
IC.19
IC.20
IC.21
IC.22
IC.23
IC.24
IC.25
IC.26
IC.27
IC.28
IC.29
IC.30
IC.31
IC.32
IC.33
IC.34
IC.35
IC.36
IC.37
IC.38
IC.39
IC.40
IC.41
IC.42
1 — IC
Contents
Professional IC Instruments
850 Professional IC
Professional IC Instrument – Introduction
IC.43
Professional IC – Detector
850 Professional IC Detector – iDetector
887 Professional UV/VIS Detector
IC.44
IC.44
Professional IC – Cation
Overwiew on 850 Professional IC instruments
850 Professional IC Cation
850 Professional IC Cation – Prep 1
850 Professional IC Cation – Prep 2
IC.45
IC.46
IC.46
IC.46
Professional IC – Anion
850
850
850
850
850
850
850
850
850
850
Professional
Professional
Professional
Professional
Professional
Professional
Professional
Professional
Professional
Professional
IC
IC
IC
IC
IC
IC
IC
IC
IC
IC
Anion
Anion
Anion
Anion
Anion
Anion
Anion
Anion
Anion
Anion
–
–
–
–
–
–
–
–
–
MSM-HC
MCS
MSM-HC – MCS
MCS – Prep 1
MSM-HC – MCS – Prep 1
MCS – Prep 2
MSM-HC – MCS – Prep 2
MCS – Prep 3
MSM-HC – MCS – Prep 3
IC.47
IC.47
IC.47
IC.47
IC.48
IC.48
IC.48
IC.48
IC.49
IC.49
Professional IC – Gradient
850
850
850
850
850
850
850
850
Professional
Professional
Professional
Professional
Professional
Professional
Professional
Professional
IC
IC
IC
IC
IC
IC
IC
IC
Cation – LP Gradient
Anion – MSM-HC – LP Gradient
Anion – MCS – LP Gradient
Anion – MSM-HC – MCS – LP Gradient
Cation – Gradient
Anion – MSM-HC – Gradient
Anion – MCS – Gradient
Anion – MSM-HC – MCS – Gradient
IC.49
IC.49
IC.50
IC.50
IC.50
IC.50
IC.51
IC.51
Professional IC – AnCat
850
850
850
850
Professional
Professional
Professional
Professional
IC
IC
IC
IC
AnCat – non-suppressed
AnCat
AnCat – MCS
AnCat – MSM-HC – MCS
IC.51
IC.51
IC.52
IC.52
Professional IC – Extension Modules
Overwiew on 872 Extension Modules
872 Extension Module IC Pump
872 Extension Module IC Module
872 Extension Module Sample Prep
872 Extension Module Liquid Handling
872 Extension Module Suppression
872 Extension Module Suppression – MCS
2 — IC
IC.53
IC.54
IC.54
IC.54
IC.54
IC.55
IC.55
Contents
Compact IC Instruments
Compact IC Instruments
Compact IC – Instruments – Introduction
Overwiew on Compact IC Instruments
IC.57
IC.58
Compact IC pro Instruments
881 Compact IC pro – Cation
881 Compact IC pro – Anion
881 Compact IC pro – Anion – MCS
IC.59
IC.59
IC.59
Compact IC plus Instruments
882 Compact IC plus – Cation
882 Compact IC plus – Anion
882 Compact IC plus – Anion – MCS
IC.60
IC.60
IC.60
Basic IC plus Instruments
883 Basic IC plus
883 Basic IC plus Package
IC.61
IC.61
3 — IC
Contents
Additional IC Componets
Alternative IC Components
Alternative IC Components – Introduction
IC.63
Heatable Reactors and Column Compartments
886 Professional Reactor
886 Professional Thermostat
IC.64
IC.64
Data Converters
891
771
771
771
Professional
IC Compact
IC Compact
IC Compact
Analog Out
Interface
Interface; MagIC Net™ Professional
Interface; MagIC Net™ Compact
IC.64
IC.65
IC.65
IC.65
Electrochemical Detectors
791 VA Detector
871 Advanced Bioscan
4 — IC
IC.66
IC.66
Contents
Professional IC – Hyphenated Technologies
Hyphenated Systems
IC – Hyphenation
IC.67
IC Hyphenated Systems
TitrIC 4 hyphenated IC and titration system
TitrIC 5 hyphenated IC and titration system
TitrIC 6 hyphenated IC and titration system
TitrIC 7 hyphenated IC and titration system
IC-MS and IC-ICP/MS Coupling
Combustion IC (Mitsubishi)
MultiTek Combustion IC (230 V)
MultiTek Combustion IC (110 V)
PILS, Particle Into Liquid Sampler
MARGA, Monitor for Aerosols and Gases in Air
IC.68
IC.68
IC.69
IC.69
IC.69
IC.70
IC.70
IC.70
IC.70
IC.71
5 — IC
Contents
Automation in Ion Chromatography
Automation
IC Automation – Introduction
Overwiew on IC Automation
858 Professional Sample Processor
858 Professional Sample Processor – Pump
858 Professional Sample Processor – Pump – Injector
889 IC Sample Center
889 IC Sample Center – cool
815 Robotic Soliprep for LC
863 Compact IC Autosampler
More sample processors for IC
6 — IC
IC.72
IC.73
IC.74
IC.75
IC.75
IC.75
IC.75
IC.76
IC.76
IC.76
IC.77
Contents
Liquid Handling in Ion Chromatography
Liquid Handling
Liquid handling in IC
IC.79
Liquid handling for IC
800 Dosino
845 Eluent Synthesizer with one Dosino
845 Eluent Synthesizer with two Dosinos
849 Level Control MF (for canisters)
849 Level Control MF (for bottles)
849 Level Control for Inline Eluent Preparation
846 Dosing Interface
IC Equipment for dialysis
IC Equipment for ultrafiltration
IC Equipment for dilution
IC Equipment for Rinsing Station to mount on Sample Processor
IC Equipment for liquid handling with Dosino
IC Equipment for Dosino Gradient
IQ/OQ Kit for IC
IC Equipment for Liquid Handling Set to PILS
Peristaltic pump, 8-channel
IC.80
IC.80
IC.81
IC.81
IC.82
IC.82
IC.82
IC.83
IC.83
IC.83
IC.83
IC.84
IC.84
IC.84
IC.84
IC.85
7 — IC
Contents
Online IC
811 Online IC Instruments
811
811
811
811
Online
Online
Online
Online
IC
IC
IC
IC
Process
Process
Process
Process
Analyzer
Analyzer
Analyzer
Analyzer
(1
(1
(2
(2
channel, 230 V)
channel, 115 V)
channels, 230 V)
channels, 115 V)
IC.87
IC.87
IC.87
IC.87
821 Compact Online IC Instruments
821 Compact Online IC Process Analyzer (230 V)
821 Compact Online IC Process Analyzer (115 V)
8 — IC
IC.89
IC.89
Contents
IC Software
Professional IC – Software
MagIC Net 2.2 Compact CD: 1 Licence
MagIC Net 2.2 Professional CD: 1 Licence
MagIC Net 2.2 Multi CD: 3 Licences
TitrIC 2.0 CD
IC.91
IC.91
IC.92
IC.92
9 — IC
Professional IC Systems
10 — IC
Professional IC Systems
850 Professional IC
Professional IC 850 – introduction
Intelligent Ion Chromatography
The 850 Professional IC is the first professional ion
chromatography system with intelligent system components that are optimally matched to one another.
The way from the sample to a precise result has now
become easier, as the system thinks for itself and
makes logical decisions on its own.
complicated calculations as well as to users who prefer
«one-button operation». Any user level is possible.
Innovation, flexibility and very simple operation result
from the intelligence of the 850 Professional IC, the
872 Extension Modules, the 858 Professional Sample
Processor and the MagIC Net™ software.
• Intelligence in the hardware of the 850 Professional IC,
- iPump
- iDetector
- iReactor
- intelligent Dosino
• Intelligence in the MagIC Net™ software
• Intelligence in the Metrosep iColumns
These are the intelligent system components that
monitor and optimise all functions and, if required, will
also document them in an FDA-compatible form. The
configuration of the system is as simple as can be, as
the components log themselves in automatically and
provide the MagIC Net™ software with all the relevant
information. The optimal operation of the 850 Professional IC and the results are monitored. If a parameter
leaves the predefined range then the user is informed
by E-mail or SMS.
The 850 Professional IC is a sophisticated and highly
efficient system and yet can be operated simply and
intuitively with the MagIC Net™ software. This applies
to experienced users and complex applications with
11 — IC
Professional IC Systems
Professional IC – ProfIC Systems
The «ProfIC» systems are packages of Professional IC
instruments and accessories tailored to the needs of a
particular group of applications. These systems feature
all the necessary components required to carry out the
respective application completely automatically. The
main components are:
-
850
850
887
858
872
800
Professional IC
Conductivity Detector
Professional UV/VIS Detector
Professional Sample Processor
Extension Module
Dosino
in the appropriate versions with the corresponding
accessories. Not included in the standard equipment
are the column, MagIC Net™, sample rack and sample
vials. This ensures maximum flexibility of the systems.
Be it the determination of anions in an analytical service laboratory with a very high sample throughput or
the detection of cations in the ultratrace range, such as
is required in nuclear power plants, the ProfIC systems
offer a custom-made solution for any ever-so-demand-
12 — IC
ing application. More than 20 systems can be called up
under http://www.professional-ic.com/. Together with
the analytical column and the software they will meet
the demands of any application.
Professional IC Systems
How to choose the right ProfIC system
Find the right system for your application in a few steps!
Step 1
Anions
Step 2
Matrix
Unloaded
Step 3
Concentration
ppt ... ppb
ppb ... ppm
Moderately loaded
with particles
Loaded with particles
Loaded with a dissolved
neutral matrix
Loaded with a dissolved
catonic matrix
Step 4
Inline Calibration
ProfIC 9 - Anion
no Inline Calibration
ProfIC 5 - Anion
Full Loop Injektion
ProfIC 1 - Anion
Partial Loop Injektion
ProfIC 15 - Anion
ppm ... %
ProfIC 4 - Anion
ppb ... ppm
ProfIC 2 - Anion
ppm ... %
ProfIC 6 - Anion
ppb ... ppm
ProfIC 3 - Anion
ppm ... %
ProfIC 7 - Anion
ppt ... ppb
ProfIC 9 - Anion
ppb ... ppm
ProfIC 8 - Anion
ppt ... ppb
ProfIC 11 - Anion
ppb ... ppm
ProfIC 10 - Anion
Anions with gadient
Anions and cations
ProfIC 12 - Anion
Unloaded
Full Loop Injektion
ProfIC 1 - AnCat
Partial Loop Injektion
ProfIC 15 - AnCat
Moderately loaded
with particles
Cations
Result
Unloaded
ProfIC 2 - AnCat
ppt ... ppb
ppb ... ppm
Moderately loaded
with particles
Loaded with particles
Loaded with a dissolved
neutral matrix
Inline Calibration
ProfIC 9 - Cation
no Inline Calibration
ProfIC 5 - Cation
Full Loop Injektion
ProfIC 1 - Cation
Partial Loop Injektion
ProfIC 15 - Cation
ppm ... %
ProfIC 4 - Cation
ppb ... ppm
ProfIC 2 - Cation
ppm ... %
ProfIC 6 - Cation
ppb ... ppm
ProfIC 3 - Cation
ppm ... %
ProfIC 7 - Cation
ppt ... ppb
ProfIC 9 - Cation
ppb ... ppm
ProfIC 8 - Cation
13 — IC
Professional IC Systems
«ProfIC 1 – Cation» – Professional IC system for
automated ion chromatography
Professional IC system applying conductivity detection.
For the fully automatic determination of cations or
anions (non-suppressed). «ProfIC 1» safely masters all
routine tasks in ion chromatography. It is simple to use
and extremely reliable.
Quality components guarantee very high sensitivity and
reproducible results. Particular attention has been given
to long service intervals; these can be monitored by the
MagIC Net™ software.
«ProfIC 1» contains intelligent system components such
as the iPump and the iDetector and provides space for
a total of three iColumns.
The 858 Professional Sample Processor provides for
sample transfer. Numerous sample racks are available
for volumes in the range 0.5...500 mL.
The «ProfIC 1» system is your reliable partner, both in
routine operation and for research and development.
14 — IC
Ordering information
ProfIC 1 - Cation
«ProfIC 1 – Cation» – Professional IC
system for automated ion chromatography
Technical information
Components
1 x 2.850.1010 850 Professional IC
1 x 2.850.9010 Conductivity Detector
1 x 2.858.0020 858 Professional Sample Processor
IC column, sample rack, sample vials as well as MagIC
Net™ have to be ordered separately according to the
specific application.
Professional IC Systems
«ProfIC 2 – Cation» – Professional IC system with
Inline Ultrafiltration
Professional IC system applying conductivity detection.
For the fully automatic determination of cations or
anions (non-suppressed) with Metrohm Inline Ultrafiltration. «ProfIC 2» masters all routine tasks in ion chromatography. It is easy to use and very reliable.
Quality system components guarantee very high sensitivity and reproducible results. Particular attention
has been given to long service intervals; these can be
monitored by the intelligent MagIC Net™ software.
«ProfIC 2» is equipped with Metrohm Inline Ultrafiltration, which reliably removes particles from the sample
and protects the analytical column from particulate
contamination. The lifetime of the column is increased
significantly. The ultrafiltration cell is equipped with a
membrane filter with a pore size of 0.2 m as standard
and is suitable for samples with a light to medium particle load. Inline Ultrafiltration works fully automatically,
which saves the time-consuming and expensive use of
syringe filters.
The ultrafiltration cell is mounted directly onto the 858
Professional Sample Processor. The bidirectional dualchannel peristaltic pump provides for sample transfer
through the ultrafiltration cell and to the Professional
IC system. The sample is continuously delivered at a
high flow rate. This delays the formation of a filter
cake and increases the working life of the membrane.
Cross contamination is kept below 0.1%.
Ordering information
ProfIC 2 - Cation
«ProfIC 2 – Cation» – Professional IC
system with inline ultrafiltration
Technical information
Components
1 x 2.850.1010 850 Professional IC
1 x 2.850.9010 850 Conductivity Detector
1 x 2.858.0020 858 Professional Sample Processor
1 x 6.5330.010 IC Equipment for ultrafiltration
IC column, sample rack, sample vials as well as MagIC
Net™ have to be ordered separately depending on
the specific application.
Numerous sample racks for volumes 0.5 ... 500 mL are
available for the 858 Professional Sample Processor.
Ultrafiltration requires at least 5 mL of sample.
«ProfIC 2» contains intelligent system components such
as the iPump and the iDetector and offers space for a
total of three iColumns.
The «ProfIC 2» system is your reliable partner, both for
routine analysis and in research and development.
15 — IC
Professional IC Systems
Metrohm Inline Ultrafiltration and dialysis
Metrohm Inline Ultrafiltration
Metrohm Inline Dialysis
Modern ion chromatography recommends all samples
to be filtered prior to injection. Separation columns
with particle sizes below 10 m require absolutely
particle-free sample solutions. Unfiltered solutions can
increase pressure on the column that in some cases
can radically reduce the lifetime of the column. Manual
filtration is usually carried out by means of disposable
filter cartridges with a pore size of 0.45 m or less.
These become clogged very quickly, particularly with
samples containing very fine particles. Sample changers with filter caps are used as an alternative. Their
pore size is often larger than that of disposable filters.
However, they are expensive and there is still a risk of
clogging.
With Metrohm Inline Ultrafiltration, which belongs to
the membrane separation techniques, these problems
no longer apply. The samples are placed directly on
the sample rack. When the samples are processed the
sample flow is channelled into the lower chamber of
the ultrafiltration cell and passes along the membrane
and into the waste container. In the upper chamber of
the cell a peristaltic pump creates a vacuum and draws
the sample solution through the ultrafiltration membrane. The filtered sample solution enters the injection
loop and is then injected. Less than 20% of the original solution is removed as filtrate, the remainder
flows directly into the waste container. This, together
with the geometrical arrangement of the cell, virtually
eliminates the formation of a filter cake that could
block the membrane. Metrohm Inline Ultrafiltration is
particularly suitable for samples with a light to medium
load, for example drinking water, surface water, wastewater, digestion solutions, extracts.
Highly polluted samples require complex and laborious
sample preparation steps before they can be analyzed.
Metrohm Inline Dialysis provides a considerable rationalization of the whole process. Samples must meet
just one condition: they must be liquid or be able to be
brought into liquid form and they need to be largely
homogeneous. Larger particles can be removed by
centrifuging, if necessary. The sample solution is then
dialyzed in the dialysis cell according to the method
patented by Metrohm (European Patent 0 820 804, US
Patent 5,861,097). Due to this special «Inline StoppedFlow Dialysis» method a virtually complete dialysis is
obtained. This means that the acceptor solution has
the same ionic concentration as the original sample
(equilibrium dialysis). The acceptor solution is then
injected directly into the ion chromatograph where it
is analyzed. Whereas in ultrafiltration the sample solution is filtered through the membrane as a result of a
difference in pressure, the driving force in dialysis is the
difference in concentration between the two sides. The
ions to be determined diffuse through the membrane,
but no sample solution is forced through the membrane. This means that no filter cake is formed that could
block the membrane. By means of this technique it
is possible to determine anions and cations even in
cutting oil emulsions, biodiesel, dairy products or body
fluids such as blood and urine.
If the system is programmed so that the next sample is
dialyzed during the current run, the total analysis takes
about the same time as direct injection.
«Stopped flow» method
An equilibrium is achieved between the acceptor solution and the sample
solution
Ultrafiltration
16 — IC
Professional IC Systems
«ProfIC 3 – Cation» – Professional IC system with
Inline Dialysis
Professional IC system applying conductivity detection.
For the fully automatic determination of cations or
anions (non-suppressed) with Metrohm Inline Dialysis.
«ProfIC 3» safely masters demanding analytical tasks
in ion chromatography. It is easy to use and extremely
reliable.
«ProfIC 3» features intelligent system components such
as the iPump and the iDetector and provides space for
a total of three iColumns.
The Professional IC system «ProfIC 3» is equipped with
«Inline Stopped Flow Dialysis», which is protected by
a Metrohm patent (European Patent 0 820 804, US
Patent 5,861,097). This fully automatic sample preparation technique effectively removes particles and colloids
from the samples. Emulsions, samples containing fats
and proteins, body fluids and strongly polluted wastewater can be reliably analyzed without damaging the
analytical column. The driving force behind dialysis is
diffusion. Only the ions and not the particles can pass
through the dialysis membrane. This increases the lifetime of the membrane and, for example, prevents oil
droplets from reaching the analytical column through
the membrane, as would be the case if filtration was
to be used.
Ordering information
ProfIC 3 - Cation
«ProfIC 3 – Cation» – Professional IC
system with Inline Dialysis
Technical information
Components
1 x 2.850.1030 850 Professional IC
1 x 2.850.9010 850 Conductivity Detector
1 x 2.858.0020 858 Professional Sample Processor
1 x 6.5330.000 IC Equipment for dialysis
IC column, sample rack, sample vials and MagIC Net™
have to be ordered separately according to the specific application.
Numerous sample racks for volumes 0.5...500 mL are
available for the 858 Professional Sample Processor.
Dialysis requires at least 10 mL of the sample.
The dialysis cell is mounted directly into the 850 Professional IC. The coordinated operation of the two
bidirectional peristaltic pumps at the 858 Professional
Sample Processor – Pump and 850 Professional IC –
Prep 1 enables the Inline Dialysis, which is controlled
by MagIC Net™.
17 — IC
Professional IC Systems
«ProfIC 4 – Cation» – Professional IC system with
Inline Dilution
Professional IC system applying conductivity detection. For the fully automatic determination of cations
or anions (non-suppressed) in concentrated solutions.
«ProfIC 4» can be used to analyze samples whose concentration is too high to be determined directly.
High ionic concentrations overload the column, which
results in poor chromatographic separation and therefore adversely affects the accuracy of the measurement.
«ProfIC 4» allows automatic Inline Dilution of any sample. Dilution takes place at an external position of the
858 Professional Sample Processor. In combination
with transfer tubing the 800 Dosino dosing system carries out the high-precision liquid handling steps.
The MagIC Net™ software controls the dilution steps
and carries out all calculations, only the dilution factor
needs to be entered in the sample table. In addition,
the software provides for intelligent dilution, i.e. dilution is carried out automatically depending on the
predefined concentration limits. The software monitors
the results and makes logical decisions.
«ProfIC 4» features intelligent system components such
as the iPump, the iDetector and the 800 Dosino and
provides space for a total of three iColumns.
The 858 Professional Sample Processor with Pump carries out the sample transfer. Numerous sample racks
for volumes 0.5...500 mL are available.
18 — IC
Ordering information
ProfIC 4 - Cation
«ProfIC 4 – Cation» – Professional IC
system with Inline Dilution
Technical information
Components
1 x 2.800.0010 800 Dosino
1 x 2.801.0010 801 Magnetic stirrer
1 x 2.850.1010 850 Professional IC
1 x 2.850.9010 850 Conductivity Detector
1 x 2.858.0020 858 Professional Sample Processor
1 x 6.3032.210 Dosing unit 10 mL
1 x 6.5330.020 IC Equipment for sample dilution
IC column, sample rack, sample vials as well as MagIC
Net™ have to be ordered separately according to the
specific application.
Professional IC Systems
«ProfIC 5 – Cation» – Professional IC system with
variable sample preconcentration
Professional IC system applying conductivity detection.
For trace analysis of cations and anions (non-supressed).
With the «ProfIC 5», concentrations down to the ppb
range (g/L) can be reliably determined. The intelligent
800 Dosino carries out the high-precision sample preconcentration on the preconcentration column, which
replaces the sample loop.
This means that it is possible to preconcentrate and
analyse more than 50 mL of the sample instead of
the 10...20 L sample used for direct injection via the
sample loop. It is also possible to calibrate the system
using the 800 Dosino dosing system. In this case it will
suffice to work with the single most concentrated standard, of which varying volumes are transferred to the
preconcentration column. This means that trace analyses are possible all the way down to the single-digit
ppb range, even in routine analysis.
«ProfIC 5» features intelligent system components
such as the iPump, the iDetector and the 800 Dosino
dosing system and provides space for a total of three
iColumns. The MagIC Net™ software monitors and
controls the functions of all components.
Ordering information
ProfIC 5 - Cation
«ProfIC 5 – Cation» – Professional IC
system with variable sample preconcentration
Technical information
Components
1 x 2.800.0010 800 Dosino
1 x 2.850.1010 850 Professional IC
1 x 2.850.9010 850 Conductivity Detector
1 x 2.858.0010 858 Professional Sample Processor
1 x 6.1014.200 Metrosep I Trap 1 column
1 x 6.1825.280 PFA transfer tubing 20 mL
1 x 6.2841.100 Rinsing station for Sample Processor
1 x 6.3032.210 Dosing unit 10 mL
1 x 6.5330.040 IC Equipment for liquid handling
IC column, preconcentration column, sample rack,
sample vials as well as MagIC Net™ have to be ordered separately according to the particular application.
The 858 Professional Sample Processor supplies the
samples. Transfer takes place with the 800 Dosino.
Numerous sample racks are available for volumes
0.5...500 mL. The minimum volume for preconcentration is 0.5 mL.
19 — IC
Professional IC Systems
«ProfIC 6 – Cation» – Professional IC system with
Inline Dilution and Ultrafiltration
Professional IC system applying conductivity detection.
For the fully automatic determination of cations or anions (non-suppressed) present in very high concentrations and whose matrix contains particles.
«ProfIC 6» works with Metrohm Inline Dilution and
Ultrafiltration. With this system it is possible to eliminate bacteria or inorganic particles from the sample
and then dilute it so far that it can be analyzed.
Automatic Inline Dilution of the sample is carried out
at an external position of the 858 Professional Sample
Processor. The 800 Dosino dosing system provides for
the high-precision liquid handling steps in combination
with a transfer tubing.
The MagIC Net™ software controls the dilution steps
and carries out all calculations, so that only the dilution factor needs to be entered in the sample table. In
addition, the software provides for intelligent dilution,
i.e. dilution takes place automatically depending on the
predefined concentration limits. The software monitors
all intelligent system components from the iColumn to
the iDetector.
The Metrohm Inline Ultrafiltration included in «ProfIC 6»
reliably removes particles from the sample, which protects the analytical column and significantly increases
its lifetime. The ultrafiltration cell is equipped with a
membrane filter with a pore size of 0.2 m as standard
and is suitable for samples with a light to medium
particle load. Inline Ultrafiltration works fully automati-
20 — IC
Ordering information
ProfIC 6 - Cation
«ProfIC 6 – Cation» – Professional IC
system with Inline Dilution and Ultrafiltration
Technical information
Components
1 x 2.800.0010 800 Dosino
1 x 2.801.0010 801 Magnetic Stirrer
1 x 2.850.1010 850 Professional IC
1 x 2.850.9010 850 Conductivity Detector
1 x 2.858.0020 858 Professional Sample Processor
1 x 6.3032.210 Dosing unit 10 mL
1 x 6.5330.010 IC Equipment for ultrafiltration
1 x 6.5330.020 IC Equipment for sample dilution
IC column, sample rack, sample vials as well as MagIC
Net™ have to be ordered separately according to the
specific application.
cally saving the time-consuming and expensive use of
syringe filters.
The 858 Professional Sample Processor with Pump carries out the sample transfer. Numerous sample racks
for volumes 0.5...500 mL are available.
Professional IC Systems
«ProfIC 7 – Cation» – Professional IC system
with Inline Dilution and Dialysis
Professional IC system applying conductivity detection.
For the fully automatic determination of cations or
anions (non-suppressed) present in high concentrations
and also in critical matrices. Emulsions, samples containing fats and proteins or strongly polluted wastewater
are not always compatible with ion chromatography,
even after an initial filtration step. This is why «ProfIC 7»
is equipped with the inline dialysis system patented
by Metrohm (European Patent 0 820 804, US-Patent
5,861,097).
In this way it is possible to determine anions and
cations even in cutting oil emulsions, biodiesel, dairy
products or body fluids such as blood and urine.
«ProfIC 7» also enables automatic Inline Dilution of the
sample. This is carried out at an external position of
the 858 Professional Sample Processor. In combination
with a transfer tubing, the 800 Dosino dosing system
carries out the high-precision liquid handling steps.
The intelligent MagIC Net™ software controls both the
dialysis and the dilution steps. MagIC Net™ carries out
all calculations, so that only the dilution factor needs
to be entered in the sample table. The software also
enables intelligent dilution, i.e. dilution takes place
automatically depending on the highest concentration
limits. The software monitors the results and makes
logical decisions.
Ordering information
ProfIC 7 - Cation
«ProfIC 7 – Cation» – Professional IC
system with Inline Dilution and Dialysis
Technical information
Components
1 x 2.800.0010 800 Dosino
1 x 2.801.0010 801 Magnetic stirrer
1 x 2.850.1030 850 Professional IC
1 x 2.850.9010 850 Conductivity Detector
1 x 2.858.0020 858 Professional Sample Processor
1 x 6.3032.210 Dosing unit 10 mL
1 x 6.5330.000 IC Equipment for dialysis
1 x 6.5330.020 IC Equipment for sample dilution
IC column, sample rack, sample vials as well as MagIC
Net™ have to be ordered separately according to the
specific application.
The 858 Professional Sample Processor provides for
sample transfer. Numerous sample racks for volumes
0.5...500 mL are available.
21 — IC
Professional IC Systems
«ProfIC 8 – Cation» – Professional IC system
with Inline Sample Preconcentration and Matrix
Elimination
The Professional IC system applying conductivity
detection. For the determination of cations or anions
(non-suppressed) in difficult matrices. «ProfIC 8» with
Metrohm Inline Sample Preconcentration and Matrix
Elimination allows chromatography unaffected by
matrix influences and guarantees a long lifetime of the
analytical column.
A small volume of the sample is transferred fully automatically to the preconcentration column. The anions
or cations are retained. The matrix can be removed in a
rinsing step. The clean sample is then injected into the
IC system.
The 850 Professional IC – Prep 2 is equipped with
an additional valve for liquid handling. The peristaltic
pump transfers the sample and the rinsing solutions.
The intelligent MagIC Net™ software controls and
monitors the system.
The 858 Professional Sample Processor provides for
sample delivery. Numerous sample racks for volumes
0.5...500 mL are available. Only small sample volumes
of about 1 mL are normally required for matrix elimination.
22 — IC
Ordering information
ProfIC 8 - Cation
«ProfIC 8 – Cation» – Professional IC
system with Inline Sample Preconcentration and Matrix Elimination
Technical information
Components
1 x 2.850.1050 850 Professional IC
1 x 2.850.9010 850 Conductivity Detector
1 x 2.858.0010 858 Professional Sample Processor
1 x 6.1602.150 Bottle neck attachment
1 x 6.1608.070 Eluent bottle 2 L, GL 45
IC column, preconcentration column, sample rack,
sample vials as well as MagIC Net™ have to be
ordered separately according to the specific application.
Professional IC Systems
«ProfIC 9 – Cation» – Professional IC system
for trace analysis with Inline Calibration, Sample
Preconcentration and Matrix Elimination
Professional IC system applying conductivity detection.
For ultratrace analysis in the lowest ppt range (ng/L) of
cations or anions (non-suppressed) in complex matrices. «ProfIC 9» with Metrohm Inline Sample Preconcentration and Matrix Elimination allows chromatography
unaffected by matrix influences and guarantees long
lifetime for the analytical column.
Metrohm Inline Calibration permits very low concentrations – in the lowest ppt range (ng/L) – to be reliably
calibrated using a single standard of higher concentration in the ppb range (g/L).
The sample is transferred to the preconcentration
column fully automatically and with high precision by
the intelligent 800 Dosino dosing system. The anions
or cations are retained. The matrix can be removed in a
rinsing step. The clean sample is then injected into the
IC system.
The 850 Professional IC – Prep 2 is equipped with
an additional valve for liquid handling. The peristaltic
pump transfers the standard solution. The intelligent
MagIC Net™ software controls and monitors the
system.
Calibration and calculation of the results as a function
of preconcentration volume is also carried out by the
MagIC Net™ software. Even if complex procedures are
involved, operating the system is perfectly easy.
Ordering information
ProfIC 9 - Cation
«ProfIC 9 – Cation» – Professional IC
system for trace analysis with Inline
Calibration, Sample Preconcentration
and Matrix elimination
Technical information
Components
1 x 2.800.0010 800 Dosino
1 x 2.850.1050 850 Professional IC
1 x 2.850.9010 850 Conductivity Detector
1 x 2.858.0010 858 Professional Sample Processor
1 x 6.1014.200 Metrosep I Trap 1 column
1 x 6.1562.130 Transfer tubing 10 mL
1 x 6.2841.100 Rinsing station for Sample Processor
1 x 6.3032.210 Dosing unit 10 mL
1 x 6.5330.040 IC Equipment for liquid handling
IC column, preconcentration column, sample rack,
sample vials as well as MagIC Net™ have to be
ordered separately according to the specific application.
The 858 Professional Sample Processor holds the samples. Numerous sample racks for volumes 0.5...500 mL
are available. Typical preconcentration volumes are
between 0.5...100 mL.
23 — IC
Professional IC Systems
«ProfIC 15 – Cation» – Professional IC system
for Partial Loop Injection
Professional IC system applying conductivity detection.
For the fully automatic determination of cations and
anions (non-suppressed) and «Partial Loop Injection».
«Partial Loop Injection» enables concentrated samples
to be injected without previous dilution as well as multipoint calibrations using just one standard solution.
«ProfIC 15» safely controls all routine tasks in ion chromatography. It is simple to use and very reliable.
Excellent system components guarantee high sensitivity
and reproducible results. Particular attention has been
given to long service intervals; these can be monitored
by the MagIC Net™ software.
«ProfIC 15» features intelligent system components
such as the iPump, the iDetector and the Dosino and
provides space for a total of three iColumns.
The 800 Dosino dosing system takes care of the sample transfer. With its high precision liquid handling, partial loop injections are performed easily and with high
reproducibility. This ensures very accurate results, for
example with calibration using just one standard.
For the 858 Professional Sample Processor numerous
sample racks are available for volumes in the range
0.5...500 mL.
The «ProfIC 15» is the perfect system configuration, both
for routine operation and research and development.
24 — IC
Ordering information
ProfIC 15 - Cation
«ProfIC 15 – Cation» – Professional IC
system for Partial Loop Injection
Technical information
Components
1 x 2.800.0010 800 Dosino
1 x 2.850.1010 850 Professional IC
1 x 2.850.9010 850 Conductivity Detector
1 x 2.858.0010 858 Professional Sample Processor
1 x 6.1825.220 PEEK sample loop 100 L
1 x 6.1831.180 PEEK capillary 0.5 mm i.D., 3 m
1 x 6.1841.000 PEEK transfer capillary 2 mL
1 x 6.2841.100 Rinsing Station for Sample Processor
1 x 6.3032.120 Dosing unit 2 mL
1 x 6.5330.040 IC Equipment for Liquid Handling
IC column, preconcentration column, sample rack,
sample vials as well as MagIC Net™ have to be ordered separately depending on the particular application.
Professional IC Systems
«ProfIC 1 – Anion» – Professional IC system
for automated ion chromatography
Professional IC system applying conductivity detection.
For the fully automatic determination of anions with
sequential suppression. «ProfIC 1» safely masters all
routine tasks in ion chromatography. It is easy to use
and extremely reliable.
Quality components guarantee high sensitivity and
reproducible results. Particular attention has been given
to long service intervals; these can be monitored by the
MagIC Net™ software.
«ProfIC 1» features intelligent system components such
as the iPump and the iDetector and provides space for
a total of three iColumns.
The anion system is equipped with sequential suppression. This unique combination of chemical and downstream CO2 suppression results in very low detection
limits. The flexibility of the carbonate/hydrocarbonate
eluent is complemented by the low background conductivity of a hydroxide eluent.
Ordering information
ProfIC 1 - Anion
«ProfIC 1 – Anion» – Professional IC
system for automated ion chromatography
Technical information
Components
1 x 2.850.2030 850 Professional IC
1 x 2.850.9010 Conductivity Detector
1 x 2.858.0020 858 Professional Sample Processor
IC column, sample rack, sample vials as well as MagIC
Net™ have to be ordered separately depending on
the specific application.
The 858 Professional Sample Processor provides for
sample transfer. Numerous sample racks are available
for volumes in the range 0.5...500 mL.
The «ProfIC 1» system is your reliable partner, both in
routine operation and for research and development.
25 — IC
Professional IC Systems
Reproducibility of the suppression
For each measurement with the Metrohm Suppressor
Module «MSM II», a fresh suppressor cartridge is used.
Thus, you can always be sure that you are working
with a cation exchanger that delivers its full performance: today, tomorrow, and even after years of
uninterrupted use. The suppressor is characterized by
its pressure stability; it is 100% solvent-resistant and
impresses with its long working life. As no sensitive
membranes are used, the suppressor reaches its equilibrium after a very short time and is then ready for
use. That is exactly the reason why we give a 10-year
warranty on the «MSM II». The Metrohm Suppressor
Module is favorably-priced and robust. Reproducibility
of measurements made with the «MSM II» is excellent
as is shown by the chromatograms:
1
2
3
4 5
7
6
30 injections, separation of standard anions on the
Metrosep A Supp 5 - 100/4.0, eluent 1.0 mmol/L NaHCO3,
3.2 mmol/L Na2CO3, flow 0.7 mL/min, loop 20 L,
suppression with the Metrohm Suppressor Module
«MSMII», regeneration with 50 mmol/L H2SO4, rinsing
with deionized water.
Ion
1
2
3
4
5
6
7
Fluoride
Chloride
Nitrite
Bromide
Nitrate
Phosphate
Sulfate
Fluoride
Chloride
Nitrite
Bromide
Nitrate
Phosphate
Sulfate
Concentration (mg/L)
0.25
0.25
0.25
0.25
0.25
0.25
0.25
Relative standard deviation in % (n=30)
0.17
0.16
0.38
0.31
0.18
0.46
0.25
26 — IC
Professional IC Systems
Sequential suppression
Sequential suppression is the combination of chemical
suppression using the «MSM II» with Metrohm CO2
Suppression «MCS». In this way anions can be detected
with carbonate/ bicarbonate eluents at the low background conductivity of hydroxide eluents.
The removal of the CO2 prevents the carbonate equilibrium from negatively affecting the peak areas. The
benefit for the user: Peak areas thus obtained are up
to 50% larger – at the same concentration and for
the same sample volume; this means lower detection
limits.
No carbonate peak also means no annoying interference with the quantification of certain analyte anions.
For example, chloride and carbonate coelute on many
polystyrene-divinylbenzene columns. By using the CO2
suppressor such problems are a thing of the past.
The virtual elimination of the injection peak improves
the determination of rapidly eluting anions, for example fluoride. Although the separation of the injection
peak and fluoride peak is already very good on polyalcohol columns, the detection limits can be improved
even further by using the CO2 suppressor. As the injection peak is practically no longer visible, considerably
larger sample volumes can also be injected.
Drinking water from Herisau (Switzerland): comparison of suppression with
«MSM II» alone (black) and with «MSM II» plus «MCS» (red).
Column:
Eluent:
Flow rate:
Metrosep A Supp 5 - 100/4.0 (6.1006.510)
3.2 mmol/L Na2CO3; 1.0 mmol/L NaHCO3
0.7 mL/min
Nr.
Ion
1
Injection peak
–
2
Fluoride
0.04
3
Chloride
7.79
4
Carbonate
5
Bromide
0.004
6
Nitrate
7.82
7
Sulfate
5.20
Conz. (mg/L)
27 — IC
Professional IC Systems
«ProfIC 2 – Anion» – Professional IC system
with Inline Ultrafiltration
Professional IC system applying conductivity detection.
For for the fully automatic determination of anions
with Metrohm Inline Ultrafiltration. «ProfIC 2» safely
masters all routine tasks in ion chromatography. It is
easy to use and extremely reliable.
Quality system components guarantee very high sensitivity and reproducible results. Particular attention
has been given to long service intervals; these can be
monitored by the intelligent MagIC Net™ software.
«ProfIC 2» is equipped with Metrohm Inline Ultrafiltration, which reliably removes particles from the sample
and effectively protects the analytical column from
contamination. The lifetime of the column is increased
significantly. The ultrafiltration cell is equipped with a
membrane filter with a pore size of 0.2 m as standard
and is suitable for samples with a light to medium particle load. Inline Ultrafiltration works fully automatically
and saves the time-consuming and expensive use of
syringe filters.
The ultrafiltration cell is mounted directly into the 858
Professional Sample Processor. The bidirectional dualchannel peristaltic pump provides for sample transfer
through the ultrafiltration cell and to the Professional
IC system. The sample is continuously delivered at a
high flow rate. This delays the formation of a filter
cake and increases the working life of the membrane.
Cross contamination is kept below 0.1%.
Ordering information
ProfIC 2 - Anion
«ProfIC 2 – Anion» – Professional IC
system with Inline Ultrafiltration
Technical information
Components
1 x 2.850.2030 850 Professional IC
1 x 2.850.9010 850 Conductivity Detector
1 x 2.858.0020 858 Professional Sample Processor
1 x 6.5330.010 IC Equipment for ultrafiltration
IC column, sample rack, sample vials as well as MagIC
Net™ have to be ordered separately depending on
the specific application.
Numerous sample racks for volumes 0.5...500 mL are
available for the 858 Professional Sample Processor.
Ultrafiltration requires at least 5 mL of the sample.
«ProfIC 2» features intelligent system components such
as the iPump and the iDetector and provides space for
a total of three iColumns.
The anion system is additionally equipped with sequential suppression. This unique combination of chemical
and downstream CO2 suppression results in very low
detection limits. The flexibility of the carbonate/hydrocarbonate eluent is complemented by the low background conductivity of a hydroxide eluent.
The «ProfIC 2» system is your reliable partner, both for
routine analysis and in research and development.
28 — IC
Professional IC Systems
«ProfIC 3 – Anion» – Professional IC system
with Inline Dialysis
Professional IC system applying conductivity detection. For the fully automatic determination of anions
with Metrohm inline dialysis. «ProfIC 3» safely masters
demanding analytical tasks in ion chromatography. It is
nevertheless simple to use and extremely reliable.
«ProfIC 3» features intelligent system components such
as the iPump and the iDetector and provides space for
a total of three iColumns.
The Professional IC system «ProfIC 3» is equipped with
«Inline Stopped Flow Dialysis», which is protected by
a Metrohm patent (European Patent 0 820 804, USPatent 5,861,097). This fully automatic sample preparation technique effectively removes particles and colloids
from the samples to be analyzed. Emulsions, samples
containing fats and proteins, body fluids and strongly polluted wastewater can be reliably determined
without damaging the analytical column. The driving
force behind dialysis is diffusion. This means that only
the ions and not the particles can pass through the
dialysis membrane. This increases the lifetime of the
membrane and, for example, prevents oil droplets from
reaching the analytical column through the membrane,
as would be the case if filtration was to be used.
The dialysis cell is mounted directly into the 850 Professional IC. The coordinated operation of the two
bidirectional peristaltic pumps at the 858 Professional
Sample Processor – Pump and 850 Professional IC
– Prep 1 enables the dialysis, which is controlled by
MagIC Net™.
Ordering information
ProfIC 3 - Anion
«ProfIC 3 – Anion» – Professional IC
system with Inline Dialysis
Technical information
Components
1 x 2.850.2110 850 Professional IC
1 x 2.850.9010 850 Conductivity Detector
1 x 2.858.0020 858 Professional Sample Processor
1 x 6.5330.000 IC Equipment for dialysis
IC column, sample rack, sample vials as well as MagIC
Net™ have to be ordered separately according to the
specific application.
The anion system is equipped with sequential suppression. Very high sensitivity is guaranteed by this
unique combination of chemical and downstream CO2
suppression. The flexibility of the carbonate eluent is
complemented by the low background conductivity of
a hydroxide eluent.
Numerous sample racks for volumes 0.5...500 mL are
available for the 858 Professional Sample Processor.
Dialysis requires at least 10 mL of the sample.
29 — IC
Professional IC Systems
«ProfIC 4 – Anion» – Professional IC system
with Inline Dilution
Professional IC system applying conductivity detection.
For the fully automatic determination of anions in concentrated solutions. «ProfIC 4» can be used to analyze
samples with concentration too high to be determined
directly.
High Ionic concentrations overload the column, which results in a poor chromatographic separation and therefore adversely affects the accuracy of the measurement.
«ProfIC 4» allows the automatic Inline Dilution of any
sample. Dilution takes place at an external position of
the 858 Professional Sample Processor. In combination
with transfer tubing the 800 Dosino carries out the
high-precision liquid handling steps.
The MagIC Net™ software controls the dilution steps
and carries out all calculations, so that only the dilution factor needs to be entered in the sample table.
Moreover, the software provides for intelligent dilution,
i.e. dilution takes place automatically depending on
the highest concentration limits. The software monitors
the results and makes logical decisions.
«ProfIC 4» features intelligent system components such
as the iPump, the iDetector and the 800 Dosino and
provides space for a total of three iColumns.
The anion system is equipped with sequential suppression. This unique combination of chemical and downstream CO2 suppression results in very low detection
limits. The flexibility of the carbonate/hydrocarbonate
30 — IC
Ordering information
ProfIC 4 - Anion
«ProfIC 4 – Anion» – Professional IC
system with Inline Dilution
Technical information
Components
1 x 2.800.0010 800 Dosino
1 x 2.801.0010 801 Magnetic stirrer
1 x 2.850.2030 850 Professional IC
1 x 2.850.9010 850 Conductivity Detector
1 x 2.858.0020 858 Professional Sample Processor
1 x 6.3032.210 Dosing unit 10 mL
1 x 6.5330.020 IC Equipment for sample dilution
IC column, sample rack, sample vials as well as MagIC
Net™ have to be ordered separately according to the
specific application.
eluent is complemented by the low background conductivity of a hydroxide eluent.
The 858 Professional Sample Processor with Pump provides for the sample transfer. Numerous sample racks
for volumes 0.5...500 mL are available.
Professional IC Systems
«ProfIC 5 – Anion» – Professional IC system
with variable sample preconcentration
Professional IC system applying conductivity detection. For trace analysis of anions. With the «ProfIC 5»,
concentrations down to the ppb range (g/L) can be
reliably determined. The intelligent 800 Dosino dosing
system carries out the high-precision sample preconcentration on the preconcentration column, which
replaces the sample loop.
This means that it is possible to preconcentrate and
analyse more than 50 mL of the sample instead of
the 10...20 L sample used for direct injection via the
sample loop. The system can be calibrated using the
800 Dosino. In this case it will suffice to work with the
single most concentrated standard, of which varying
volumes are transferred to the preconcentration
column. This allows trace analyis right down to the the
single digit ppb range even in routine analysis.
«ProfIC 5» features intelligent system components
such as the iPump, the iDetector and the 800 Dosino
dosing system and provides space for a total of three
iColumns. The MagIC Net™ software monitors and
controls the functions of all components.
The anion system is equipped with sequential suppression. This unique combination of chemical and downstream CO2 suppression enables very low detection
limits. The flexibility of the carbonate/hydrocarbonate
eluent is complemented by the low background conductivity of a hydroxide eluent. With the preconcentration technique carbonate interference is practically
eliminated.
Ordering information
ProfIC 5 - Anion
«ProfIC 5 – Anion» – Professional IC
system with variable sample preconcentration
Technical information
Components
1 x 2.800.0010 800 Dosino
1 x 2.850.2030 850 Professional IC
1 x 2.850.9010 850 Conductivity Detector
1 x 2.858.0010 858 Professional Sample Processor
1 x 6.1014.200 Metrosep I Trap 1 column
1 x 6.1562.130 PEEK transfer tubing 10 mL
1 x 6.2841.100 Rinsing station for Sample Processor
1 x 6.3032.210 Dosing unit 10 mL
1 x 6.5330.040 IC Equipment for liquid handling
IC column, preconcentration column, sample rack,
sample vials as well as MagIC Net™ have to be ordered
separately according to the particular application.
The 858 Professional Sample Processor supplies the
samples. Transfer is carried out by the 800 Dosino
dosing system. Numerous sample racks are available
for volumes 0.5...500 mL. The minimum volume for
preconcentration is 0.5 mL.
31 — IC
Professional IC Systems
«ProfIC 6 – Anion» – Professional IC system
with Inline Dilution and Ultrafiltration
Professional IC system applying conductivity detection.
For the fully automatic determination of anions in very
high concentrations in matrices containing particles.
«ProfIC 6» works with Metrohm Inline Dilution and
Ultrafiltration. This system enables users to dilute the
sample and eliminate bacteria or inorganic particles
prior to analysis.
Automatic Inline Dilution of the sample is carried out
at an external position of the 858 Professional Sample
Processor. The 800 Dosino dosing system carries out
the high-precision liquid handling steps.
The MagIC Net™ software controls the dilution steps
and provides for all calculations; only the dilution factor
needs to be entered in the sample table. In addition,
the software provides for intelligent dilution, i.e. dilution takes place automatically depending on the predefined concentration limits. The software monitors all
intelligent system components from the iColumn to the
iDetector.
The Metrohm Inline Ultrafiltration included in «ProfIC 6»
reliably removes particles from the sample protecting
the analytical column and increasing its lifetime significantly. The ultrafiltration cell is equipped with a membrane filter with a pore size of 0.2 m as standard and
is suitable for samples with a light to medium particle load. Inline Ultrafiltration works fully automatically
saving the time-consuming and expensive use of
syringe filters.
Ordering information
ProfIC 6 - Anion
«ProfIC 6 – Anion» – Professional IC
system with Inline Dilution and Ultrafiltration
Technical information
Components
1 x 2.800.0010 800 Dosino
1 x 2.801.0010 801 Magnetic Stirrer
1 x 2.850.2030 850 Professional IC Anion
1 x 2.850.9010 850 Conductivity Detector
1 x 2.858.0020 858 Professional Sample Processor
1 x 6.3032.210 Dosing unit 10 mL
1 x 6.5330.010 IC Equipment for ultrafiltration
1 x 6.5330.020 IC Equipment for sample dilution
IC column, sample rack, sample vials as well as MagIC
Net™ have to be ordered separately according to the
specific application.
The anion system is equipped with sequential suppression. Very high sensitivity is achieved by this unique
combination of chemical and downstream CO2 suppression. The flexibility of the carbonate/hydrocarbonate eluent is complemented by the low background
conductivity of a hydroxide eluent.
The 858 Professional Sample Processor with Pump carries out the sample transfer. Numerous sample racks
for volumes 0.5...500 mL are available.
32 — IC
Professional IC Systems
«ProfIC 7 – Anion» – Professional IC system
with Inline Dilution and Dialysis
Professional IC system applying conductivity detection.
For the fully automatic determination of anions in
high concentrations and in critical matrices. Emulsions, samples containing fats and proteins or strongly
polluted wastewater are not always compatible with
ion chromatography, even after filtration. This is why
«ProfIC 7» is equipped with the Inline Dialysis system
patented by Metrohm (European Patent 0 820 804,
US-Patent 5,861,097).
In this way it is possible to determine anions and
cations even in cutting oil emulsions, dairy products or
body fluids such as blood and urine.
«ProfIC 7» also enables automatic Inline Dilution of the
sample. This takes place at an external position of the
858 Professional Sample Processor. The 800 Dosino
carries out the high-precision liquid handling steps.
The intelligent MagIC Net™ software controls both the
dialysis and the dilution steps. MagIC Net™ provides
for all calculations; only the dilution factor needs to be
entered in the sample table. In addition, the software
provides for intelligent dilution, i.e. dilution takes place
automatically depending on the predefined concentration limits. The software monitors the results and
makes logical decisions.
The anion system is equipped with sequential suppression. Very high sensitivity is achieved by this unique
combination of chemical and downstream CO2 sup-
Ordering information
ProfIC 7 - Anion
«ProfIC 7 – Anion» – Professional IC
system with Inline Dilution and Dialysis
Technical information
Components
1 x 2.800.0010 800 Dosino
1 x 2.801.0010 801 Magnetic Stirrer
1 x 2.850.2110 850 Professional IC
1 x 2.850.9010 850 Conductivity Detector
1 x 2.858.0020 858 Professional Sample Processor
1 x 6.3032.210 Dosing unit 10 mL
1 x 6.5330.000 IC Equipment for dialysis
1 x 6.5330.020 IC Equipment for sample dilution
IC column, sample rack, sample vials as well as MagIC
Net™ have to be ordered separately according to the
specific application.
pression. The flexibility of the carbonate/hydrocarbonate eluent is complemented by the low background
conductivity of a hydroxide eluent.
The 858 Professional Sample Processor with Pump carries out the sample transfer. Numerous sample racks
for volumes 0.5...500 mL are available.
33 — IC
Professional IC Systems
«ProfIC 8 – Anion» – Professional IC system
with Inline Sample Preconcentration and Matrix
Elimination
Professional IC system applying conductivity detection.
For the determination of anions in difficult matrices.
«ProfIC 8» with Metrohm Inline Sample Preconcentration and Matrix elimination allows chromatography unaffected by matrix influences and guarantees
a long lifetime of the analytical column.
A small volume of the sample is transferred fully automatically to the preconcentration column. The anions
are retained. The matrix can be removed in a rinsing
step. The clean sample is then injected into the IC system.
The 850 Professional IC – Prep 2 is equipped with
an additional valve for liquid handling. The peristaltic
pump transfers the sample and the rinsing solutions.
The intelligent MagIC Net™ software controls and
monitors the system.
The anion system is equipped with sequential suppression. This unique combination of chemical and downstream CO2 suppression results in very low detection
limits. The flexibility of the carbonate/hydrocarbonate
eluent is complemented by the low background conductivity of a hydroxide eluent. With the preconcentration technique carbonate interference is practically
eliminated.
The 858 Professional Sample Processor provides for
sample delivery. Numerous sample racks for volumes
0.5...500 mL are available. Only small sample volumes
of about 1 mL are normally required for Matrix Elimination.
34 — IC
Ordering information
ProfIC 8 - Anion
«ProfIC 8 – Anion» – Professional IC
system with Inline Sample Preconcentration and Matrix elimination
Technical information
Components
1 x 2.850.2150 850 Professional IC Anion
1 x 2.850.9010 850 Conductivity Detector
1 x 2.858.0010 858 Professional Sample Processor
1 x 6.1602.150 Bottle neck attachment
1 x 6.1608.070 Eluent bottle 2 L, GL 45
IC column, preconcentration column, sample rack,
sample vials as well as MagIC Net™ have to be
ordered separately according to the specific application.
Professional IC Systems
«ProfIC 9 – Anion» – Professional IC system
for trace analysis with Inline Calibration, Sample
Preconcentration and Matrix Elimination
Professional IC system applying conductivity detection.
For ultratrace analysis in the lowest ppt range (ng/L) of
anions in complex matrices. «ProfIC 9» with Metrohm
Inline Sample Preconcentration and Matrix Elimination
allows chromatography unaffected by matrix influences
and guarantees that the analytical column has a long
working life.
Metrohm Inline Calibration permits very low concentrations – in the lowest ppt range – to be reliably calibrated using a single standard of higher concentration
– in the ppb range.
The sample is transferred to the preconcentration column
fully automatically and with high precision by the intelligent 800 Dosino dosing system. The anions are retained.
The matrix can be removed in a rinsing step. The clean
sample is then injected into the IC system.
The 850 Professional IC – Prep 2 is equipped with an
additional valve for liquid handling. The peristaltic pump
transfers the standard solution. The intelligent MagIC
Net™ software controls and monitors the system.
Calibration and calculation of the results as a function
of preconcentration volume are also provided by the
MagIC Net™ software. Even if complex procedures are
involved, operating the system is perfectly simple.
The anion system is equipped with sequential suppression. Very high sensitivity is achieved by this unique
combination of chemical and downstream CO2 sup-
Ordering information
ProfIC 9 - Anion
«ProfIC 9 – Anion» – Professional IC
system for trace analysis with Inline
Calibration, Sample Preconcentration
and Matrix Elimination
Technical information
Components
1 x 2.800.0010 800 Dosino
1 x 2.850.2150 850 Professional IC
1 x 2.850.9010 850 Conductivity Detector
1 x 2.858.0010 858 Professional Sample Processor
1 x 6.1014.200 Metrosep I Trap 1 Column
1 x 6.1562.130 PEEK Transfer tubing 10 mL
1 x 6.2841.100 Rinsing station for Sample Processor
1 x 6.3032.210 Dosing unit 10 mL
1 x 6.5330.040 IC Equipment for liquid handling
IC column, preconcentration column, sample rack,
sample vials as well as MagIC Net™ have to be
ordered separately according to the specific application.
pression. The flexibility of the carbonate/hydrocarbonate eluent is complemented by the low background
conductivity of a hydroxide eluent. With the preconcentration technique carbonate interference is practically eliminated.
The 858 Professional Sample Processor holds the samples.
Numerous sample racks for volumes 0.5...500 mL are
available. Typical preconcentration volumes are between
0.5...100 mL.
35 — IC
Professional IC Systems
«ProfIC 10 – Anion» – Professional IC system
with Inline Sample Preconcentration,
Matrix Elimination and Matrix Neutralisation
Professional IC system applying conductivity detection.
For the determination of anions in difficult matrices.
«ProfIC 10» with Metrohm Inline Sample Preconcentration, Matrix Neutralisation and Matrix Elimination
allows chromatography unaffected by matrix influences
and guarantees that the analytical column has a long
lifetime.
A small volume of the sample is transferred fully automatically to the preconcentration column. On its way it
passes through the sample preparation module, where
an almost complete cation exchange takes place. This
means that it is possible to neutralise both acids and
alkalis. The matrix is then removed from the preconcentration column in a rinsing step and the clean and
pH-neutral sample injected into the IC system.
For liquid handling, the 858 Professional Sample Processor – Pump – Injector is equipped with an additional valve. An additional peristaltic pump transfers the
sample and rinsing solutions. The intelligent MagIC
Net™ software controls and monitors the system.
«ProfIC 10» is equipped with sequential suppression.
Very high sensitivity is achieved by this unique combination of chemical and downstream CO2 suppression.
The flexibility of the carbonate/hydrocarbonate eluent
is complemented by the low background conductivity
of a hydroxide eluent. With the preconcentration technique, carbonate interference is practically eliminated.
36 — IC
Ordering information
ProfIC 10 - Anion
«ProfIC 10 – Anion» – Professional IC
system with Inline Sample Preconcentration, Matrix Elimination and Matrix
Neutralisation
Technical information
Components
1 x 2.850.2190 850 Professional IC Anion
1 x 2.850.9010 850 Conductivity Detector
1 x 2.858.0030 858 Professional Sample Processor
1 x 6.1602.150 Bottle neck attachment
1 x 6.1608.070 Eluent bottle 2 L, GL 45
1 x 6.1825.230 PEEK sample loop 10 L
IC column, preconcentration column, sample rack,
sample vials as well as MagIC Net™ have to be
ordered separately according to the particular application.
«ProfIC 10» features intelligent system components
such as the iPump and the iDetector and provides
space for a total of three iColumns.
The 858 Professional Sample Processor – Pump – Injector provides for sample delivery. Numerous sample
racks for volumes 0.5...500 mL are available. Only
small sample volumes of about 1 mL are normally
required for Matrix Elimination and Neutralisation.
Professional IC Systems
«ProfIC 11 – Anion» – Professional IC system
for trace analysis with Inline Calibration, Sample
Preconcentration and Matrix Elimination
Professional IC system applying conductivity detection.
For ultratrace analysis of anions in complex matrices.
«ProfIC 11» with Metrohm Inline Neutralisation, Sample
Preconcentration and Matrix Elimination allows chromatography unaffected by matrix influences and guarantees al long lifetime of the analytical column.
Metrohm Inline Calibration permits very low concentrations – in the ppt range (ng/L) – to be reliably calibrated using a single standard of higher concentration – in
the ppb range (g/L).
The sample is transferred to the preconcentration
column fully automatically and with high precision by
the intelligent 800 Dosino dosing system. On its way it
passes through the sample preparation module, where
complete cation exchange takes place. This means
that it is possible to neutralise both acids and bases.
The matrix is then removed from the preconcentration
column in a rinsing step. The pH-neutral and matrixfree sample is then injected into the IC system. The
preconcentration becomes possible as a result of the
neutralisation of the sample.
The 850 Professional IC – Prep 3 is equipped with a
sample preparation module. Sample and rinsing solution are provided by the 800 Dosino. A valve on the
858 Professional Sample Processor switches between
sampling and sample transfer. The 872 Extension
Module is used for Inline Calibration. The intelligent
MagIC Net™ software controls and monitors the system.
Ordering information
ProfIC 11 - Anion
«ProfIC 11 – Anion» – Professional IC
system for trace analysis with Inline
Calibration, Sample Preconcentration
and Matrix Elimination
Technical information
Components
1 x 2.800.0010 800 Dosino
1 x 2.850.2190 850 Professional IC
1 x 2.850.9010 850 Conductivity Detector
1 x 2.858.0030 858 Professional Sample Processor
1 x 2.872.0050 872 Extension Module Sample Prep
1 x 6.1014.200 Metrosep I Trap 1 Column
1 x 6.1562.130 PEEK Transfer tubing 10 mL
1 x 6.2841.100 Rinsing station for Sample Processor
1 x 6.3032.150 Dosing unit 5 mL
1 x 6.5330.040 IC Equipment for liquid handling
IC column, preconcentration column, sample rack,
sample vials as well as MagIC Net™ have to be
ordered separately according to the specific application.
Calibration and calculation of the results as a function
of preconcentration volume are also provided by the
MagIC Net™ software. Different sample volumes can
be conveniently entered in the sample table. Even if
complex procedures are involved, operating the system
is perfectly easy.
«ProfIC 11» features intelligent system components
such as the iPump, the iDetector and the Dosino and
provides space for a total of three iColumns. The
system is equipped with sequential suppression.
The 858 Professional Sample Processor – Pump – Injector provides for sample delivery. Numerous sample
racks for volumes 0.5...500 mL are available.
37 — IC
Professional IC Systems
«ProfIC 12 – Anion» – Professional IC gradient
system
Professional IC system applying conductivity detection.
For the determination of anions with a binary highpressure gradient. In addition to step gradients, this
system can be used to run any linear, convex or concave gradients to work in a time-optimized way.
«ProfIC 12» is equipped with two high-pressure pumps
and a very effective passive mixing device. The 872
Extension Module IC Pump can be used to upgrade the
system to a quaternary gradient.
«ProfIC 12» works with sequential suppression. This
unique combination of chemical and downstream CO2
suppression results in very low detection limits. The flexibility of the carbonate/hydrocarbonate eluent is complemented by the low background conductivity of a
hydroxide eluent. The removal of carbon dioxide additionally reduces baseline drift during the gradient run.
The MagIC Net™ software is used for controlling the
system and programming the gradient. All system functions, from monitoring the service interval to calibration, can be monitored by MagIC Net™.
«ProfIC 12» features intelligent system components
such as two iPumps and the iDetector and provides
space for a total of three iColumns.
The 858 Professional Sample Processor – Pump provides for for sample delivery. Numerous sample racks for
volumes 0.5...500 mL are available.
38 — IC
Ordering information
ProfIC 12 - Anion
«ProfIC 12 – Anion» – Professional IC
gradient system
Technical information
Components
1 x 2.850.2220 850 Professional IC Anion
1 x 2.850.9010 850 Conductivity Detector
1 x 2.858.0020 858 Professional Sample Processor
IC column, sample rack, sample vials as well as MagIC
Net™ have to be ordered separately according to the
particular application.
Professional IC Systems
«ProfIC 15 – Anion» – Professional IC system
for Partial Loop Injection
Professional IC system applying conductivity detection.
For the fully automatic determination of anions with
sequential suppression and Partial Loop Injection capability. «Partial Loop Injection» enables concentrated
samples to be injected without previous dilution as well
as multipoint calibrations using just one standard solution. «ProfIC 15» safely controls all routine tasks in ion
chromatography. It is easy to use and very reliable.
Excellent system components guarantee high sensitivity
and reproducible results. Particular attention has been
given to long service intervals; these can be monitored
by the MagIC Net™ software.
«ProfIC 15» features intelligent system components
such as the iPump, the iDetector and the 800 Dosino
and provides space for a total of three iColumns.
The anion system is equipped with sequential suppression. This unique combination of chemical and downstream CO2 suppression results in very low detection
limits. The flexibility of the carbonate/hydrocarbonate
eluent can thus be combined with the low background
conductivity of a hydroxide eluent.
The 800 Dosino dosing system provides for the sample
transfer. Due to its high precision liquid handling, Partial Loop Injections are performed easily and with high
reproducibility. This ensures very accurate results, for
example with calibration using one single solution.
Ordering information
ProfIC 15 - Anion
«ProfIC 15 – Anion» – Professional IC
system for Partial Loop Injection
Technical information
Components
1 x 2.800.0010 800 Dosino
1 x 2.850.2030 850 Professional IC Anion
1 x 2.850.9010 850 Conductivity Detector
1 x 2.858.0010 858 Professional Sample Processor
1 x 6.1825.220 PEEK sample loop 100 L
1 x 6.1831.180 PEEK-capillary 0.5 mm i.D., 3 m
1 x 6.1841.000 PEEK transfer capillary 2 mL
1 x 6.2841.100 Rinsing Station for Sample Processor
1 x 6.3032.120 Dosing unit 2 mL
1 x 6.5330.040 IC Equipment for Liquid Handling
IC column, sample rack, sample vials as well as MagIC
Net™ have to be ordered separately according to the
particular application.
For the 858 Professional Sample Processor numerous
sample racks are available for volumes in the range
0.5...500 mL.
The «ProfIC 15» system is your reliable partner, both for
routine operation and in research and development.
39 — IC
Professional IC Systems
«ProfIC 1 – AnCat» – Professional IC system
for automated ion chromatography
Very compact Professional IC system applying conductivity detection for the fully automatic determination
of anions and cations. With «ProfIC 1 – AnCat» anions
and cations can be determined both in parallel as well
as independently. Both systems use the same 858 Professional Sample Processor with pump, which is controlled by the MagIC Net™ software.
Ordering information
ProfIC 1 - AnCat
«ProfIC 1 – AnCat» – Professional IC
system for automated ion chromatography
The «ProfIC 1 – AnCat» safely performs all routine tasks
in ion chromatography. It is simple to operate and very
reliable. Excellent system components guarantee low
detection limits and reproducible results. Particular
attention has been given to long service intervals; these
can be monitored with the MagIC Net™ software.
Technical information
Components
1 x 2.850.3030 850 Professional IC
2 x 2.850.9010 850 Conductivity Detector
1 x 2.858.0020 858 Professional Sample Processor
The anion system is equipped with sequential suppression. This unique combination of chemical and downstream CO2 suppression results in very low detection
limits. The flexibility of the carbonate/hydrocarbonate
eluent is complemented by the low background conductivity of a hydroxide eluent.
«ProfIC 1 – AnCat» features two iPumps as well as
two iDetectors and provides space for a total of three
iColumns in two different temperature ranges.
The 858 Professional Sample Processor – Pump provides for the sample transfer. Numerous sample racks for
volumes 0.5...500 mL are available.
40 — IC
IC column, sample rack, sample vials as well as MagIC
Net™ have to be ordered separately according to the
particular application.
The «ProfIC 1-AnCat» system is your reliable partner,
both for routine operation and in research and development.
Professional IC Systems
«ProfIC 2 – AnCat» – Professional IC system
with Inline Ultrafiltration
The very compact Professional IC system applying conductivity detection for the fully automatic determination of anions and cations with Metrohm Inline Ultrafiltration. With «ProfIC 2 – AnCat» anions and cations
can be determined both in parallel as well as independently in order to save time. Both systems use the
same 858 Professional Sample Processor with – pump,
which is controlled by the MagIC Net™ software.
The «ProfIC 2 – AnCat» performs all routine tasks in
ion chromatography. It is simple to operate and very
reliable. Excellent system components guarantee low
detection limits and reproducible results. Particular
attention has been given to long service intervals; these
can be monitored with the MagIC Net™ software.
«ProfIC 2 – AnCat» is equipped with Metrohm Inline
Ultrafiltration, which reliably removes particles from
the sample protecting the analytical column particulate
contamination. The lifetime of the column is significantly increased. The ultrafiltration cell is equipped with
a membrane filter with a pore size of 0.2 m as standard and is suitable for samples with a light to medium
particle load. Inline Ultrafiltration works fully automatically saving the time-consuming and expensive use of
syringe filters.
The ultrafiltration cell is mounted directly into the 858
Professional Sample Processor. The bidirectional dualchannel peristaltic pump carries out the sample transfer
through the ultrafiltration cell and to the Professional
IC system.
Ordering information
ProfIC 2 - AnCat
«ProfIC 2 – AnCat» – Professional IC
system with Inline Ultrafiltration
Technical information
Components
1 x 2.850.3030 850 Professional IC
2 x 2.850.9010 850 Conductivity Detector
1 x 2.858.0020 858 Professional Sample Processor
1 x 6.5330.010 IC Equipment for ultrafiltration
IC column, sample rack, sample vials as well as MagIC
Net™ have to be ordered separately according to the
particular application.
The anion system is additionally equipped with sequential suppression. This unique combination of chemical
and downstream CO2 suppression results in very low
detection limits. The flexibility of the carbonate/hydrocarbonate eluent is complemented by the low background conductivity of a hydroxide eluent.
«ProfIC 2 – AnCat» features two iPumps as well as two
iDetectors and provides space for a total of three iColumns in two different temperature ranges.
Numerous sample racks for volumes 0.5...500 mL are
available. Ultrafiltration requires a sample volume of at
least 5 mL.
The «ProfIC 2-AnCat» system is your reliable partner,
both for routine operation and in research and development.
41 — IC
Professional IC Systems
«ProfIC 15 – AnCat» – Professional IC system
for Partial Loop Injection
Very compact Professional IC system applying conductivity detection for the fully automatic determination
of anions with sequential suppression and cations with
Partial Loop Injection capability.
«Partial Loop Injection» allows concentrated samples
to be injected without previous dilution as well as multipoint calibrations using just one standard solution.
«ProfIC 15» safely controls all routine tasks in ion chromatography. It is simple to use and very flexible.
Excellent system components guarantee high sensitivity
and reproducible results. Particular attention has been
given to long service intervals; these can be monitored
by the MagIC Net™ software.
«ProfIC 15 – AnCat» features two iPumps, two Dosinos as well as two iDetectors and provides space for
a total of three iColumns in two different temperature
ranges.
The anion system is equipped with sequential suppression. This unique combination of chemical and downstream CO2 suppression results in very low detection
limits. The flexibility of the carbonate/hydrocarbonate
eluent is complemented by the low background conductivity of a hydroxide eluent.
The 800 Dosino dosing system provides for the sample transfer. Due to its high precision liquid handling,
Partial Loop Injections are performed easily and with
high reproducibility. This ensures very accurate results,
Ordering information
ProfIC 15 - AnCat
«ProfIC 15 – AnCat» – Professional IC
system for partial loop injection
Technical information
Components
2 x 2.800.0010 800 Dosino
1 x 2.850.3030 850 Professional IC
2 x 2.850.9010 850 Conductivity Detector
1 x 2.858.0010 858 Professional Sample Processor
1 x 6.1825.220 PEEK sample loop 100 L
1 x 6.1831.180 PEEK-capillary 0.5 mm i.D., 3 m
1 x 6.1841.000 PEEK transfer capillary 2 mL
1 x 6.2744.290 T-connector with holder
1 x 6.2841.100 Rinsing Station for Sample Processor
1 x 6.3032.120 Dosing unit 2 mL
1 x 6.5330.040 IC Equipment for Liquid Handling
IC column, sample rack, sample vials as well as MagIC
Net™ have to be ordered separately according to the
particular application.
for example when calibrating using one single standard
solution.
For the 858 Professional Sample Processor numerous
sample racks are available for volumes in the range
0.5...500 mL.
The «ProfIC 15» is the perfect system configuration, both
for routine operation and research and development.
42 — IC
Professional IC Instruments
Professional IC Instruments
Professional IC Instrument – Introduction
850 Professional IC – intelligent ion chromatography
Configuration: configuration of the system could not
be easier, as the components log themselves in automatically and all the relevant information is available to
the MagIC Net™ software.
Monitoring: the system monitors and optimises all
functions and, if required, documents them in an FDAcompatible form. Optimal operation of the 850 Professional IC and results are monitored. If a parameter is
outside the predefined range, then the user is informed
by E-mail or SMS.
Free choice of detection mode:
The detection mode can be choosen. Therefore no
detector is included in the scope of delivery.
-
Intelligent pump: iPump
Intelligent detector: iDetector
Intelligent column: iColumn
Intelligent liquid handling with Dosinos
Extension Module
Inline sample preparation: the way from sample preparation to precise result has become shorter, as now
even complex sample preparation steps can be carried
out inline and automatically. The system automatically optimises sample preconcentration or dilution as
required.
43 — IC
Professional IC Instruments
850 Professional IC – detectors
850 Professional IC Detector – iDetector
(2.850.9010)
Compact and intelligent high performance conductivity detector for intelligent IC Instruments. Outstanding
temperature stability, the complete signal processing
within the protected detector block and the latest
generation of «DSP» – Digital Signal Processing – guarantee the highest precision of the measurement. No
change of measuring ranges – not even automatic – is
required due to the dynamic working range.
887 Professional UV/VIS Detector
(2.887.0010)
The 887 Professional UV/VIS Detector is an alternative
to the conductivity detector and expands the family
of intelligent Metrohm detectors. It allows the reliable
quantification of components that absorb ultraviolet or
visible light. Detection is by a diode array.
44 — IC
Professional IC Instruments
Overwiew on 850 Professional IC instruments
Comparison of the different 850 Professional IC instruments
2.850.1010
2.850.1030
2.850.1050
2.850.1210
2.850.1220
2.850.2010
2.850.2030
2.850.2050
2.850.2070
2.850.2110
2.850.2120
2.850.2140
2.850.2150
2.850.2180
2.850.2190
2.850.2210
2.850.2220
2.850.2230
2.850.2240
2.850.2250
2.850.2260
2.850.3000
2.850.3010
2.850.3030
2.850.3040
Professional IC Cation
Professional IC Cation Prep 1
Professional IC Cation Prep 2
Professional IC Cation LP Gradient
Professional IC Cation Gradient
Professional IC Anion
Professional IC Anion MCS
Professional IC Anion MSM-HC
Professional IC Anion MSM-HC MCS
Professional IC Anion MCS Prep 1
Professional IC Anion MSM-HC MCS Prep 1
Professional IC Anion MSM-HC MCS Prep 2
Professional IC Anion MCS Prep 2
Professional IC Anion MSM-HC MCS Prep 3
Professional IC Anion MCS Prep 3
Professional IC Anion MCS LP Gradient
Professional IC Anion MCS Gradient
Professional IC Anion MSM-HC MCS LP Gradient
Professional IC Anion MSM-HC MCS Gradient
Professional IC Anion MSM-HC LP Gradient
Professional IC Anion MSM-HC Gradient
Professional IC AnCat non-suppressed
Professional IC AnCat
Professional IC AnCat MCS
Professional IC AnCat MSM-HC MCS
Sample preparation
Prep 1
Prep 2
Prep 3
PP +
PP +
PP
Valve
SPM
Gradient
HPG
LPG
LPiPump
Device
iPump +
Valve
MSM
PP +
MSM
Suppression
MSM-HC
PP +
MSM-HC
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes
yes, 2x
yes, 2x
yes
yes, 2x
yes
yes
yes, 2x
yes
yes
IC
Module
MCS
MCS
45 — IC
Professional IC Instruments
850 Professional IC – instruments
for cation determination
850 Professional IC Cation
(2.850.1010)
The 850 Professional IC Cation is an intelligent ion
chromatography system for the determination of
anions or cations without suppression. It may be combined with different detector types.
850 Professional IC Cation – Prep 1
(2.850.1030)
The 850 Professional IC Cation – Prep 1 is an intelligent
ion chromatography system for the determination of
anions or cations without suppression in combination
with sample preparation techniques such as Ultrafiltration and Dialysis. It may be combined with different
detector types.
850 Professional IC Cation – Prep 2
(2.850.1050)
The 850 Professional IC Cation – Prep 2 is an intelligent
ion chromatography system for the determination of
anions or cations without suppression after sample
preparation. The system is suitable for the integration
of Metrohm Iinline Sample Preconcentration, matrix
elimination or inline calibration. It may be combined
with different detector types.
46 — IC
Professional IC Instruments
850 Professional IC instruments
for anion determination
850 Professional IC Anion (2.850.2010)
The 850 Professional IC Anion is an intelligent ion chromatography system for the determination of anions
with chemical suppression. It may be combined with
different detector types.
850 Professional IC Anion – MSM-HC
(2.850.2050)
The 850 Professional IC Anion – MSM-HC is an intelligent ion chromatography system for the determination
of anions with high-capacity chemical suppression. It
may be combined with different detector types.
850 Professional IC Anion – MCS
(2.850.2030)
The 850 Professional IC Anion – MCS is an intelligent
ion chromatography system for the determination of
anions with sequential suppression. It may be combined
with different detector types.
850 Professional IC Anion – MSM-HC
– MCS (2.850.2070)
The 850 Professional IC Anion – MSM-HC – MCS is an
intelligent ion chromatography system for the determination of anions with high-capacity sequential suppression. It may be combined with different detector types.
47 — IC
Professional IC Instruments
850 Professional IC Anion – MCS
– Prep 1 (2.850.2110)
The 850 Professional IC Anion – MCS – Prep 1 is an
intelligent ion chromatography system for the determination of anions with sequential suppression in
combination with Metrohm Inline Sample Preparation
Techniques such as Ultrafiltration or Dialysis. It may be
combined with different detector types.
850 Professional IC Anion – MSM-HC –
MCS – Prep 1 (2.850.2120)
The 850 Professional IC Anion – MSM-HC – MCS –
Prep 1 is an intelligent ion chromatography system for
the determination of anions with high-capacity sequential suppression in combination with Metrohm Inline
Sample Preparation Techniques such as Ultrafiltration
or Dialysis. It may be combined with different detector
types.
850 Professional IC Anion – MCS –
Prep 2 (2.850.2150)
The 850 Professional IC Anion – MCS – Prep 2 is an
intelligent ion chromatography system for the determination of anions with sequential suppression. At the
same time it allows fully automatic sample preparation
with Metrohm Inline Sample Preconcentration, Inline
Matrix Elimination or Inline Calibration. It may be combined with different detector types.
850 Professional IC Anion – MSM-HC
– MCS – Prep 2 (2.850.2140)
The 850 Professional IC Anion – MSM-HC – MCS –
Prep 2 is an intelligent ion chromatography system
for the determination of anions with high-capacity
sequential suppression. At the same time it allows fully
automatic sample preparation with Metrohm Inline
Sample Preconcentration, Inline Matrix Elimination or
Inline Calibration. It may be combined with different
detector types.
48 — IC
Professional IC Instruments
850 Professional IC Anion – MCS
– Prep 3 (2.850.2190)
The 850 Professional IC Anion – MCS – Prep 3 is
an intelligent ion chromatography system for the
determination of anions with sequential suppression
with simultaneous Metrohm Inline Neutralization or
Metrohm Inline Cation Removal. It may be combined
with different detector types.
850 Professional IC Anion – MSM-HC
– MCS – Prep 3 (2.850.2180)
The 850 Professional IC Anion – MSM-HC – MCS –
Prep 3 is an intelligent ion chromatography system for
the determination of anions with high-capacity sequential suppression with simultaneous Metrohm Inline
Neutralization or Metrohm Inline Cation Removal. It
may be combined with different detector types.
850 Professional IC instruments with gradient
850 Professional IC Cation – LP Gradient (2.850.1210)
The 850 Professional IC Cation – LP Gradient is an
intelligent ion chromatography system with low pressure gradient but without suppression. This instrument
may be combined with any separation and detection
mode requiring no suppression. It may be combined
with different detector types.
850 Professional IC Anion – MSM-HC
– LP Gradient (2.850.2250)
The 850 Professional IC Anion – MSM-HC – LP Gradient is an intelligent ion chromatography system for the
determination of anions using high-capacity chemical
suppression and low-pressure gradient. It may be combined with different detector types.
49 — IC
Professional IC Instruments
850 Professional IC Anion – MCS – LP
Gradient (2.850.2210)
The 850 Professional IC Anion – MCS – LP Gradient
is an intelligent ion chromatography system for the
determination of anions using sequential suppression
and low-pressure gradient. It may be combined with
different detector types.
850 Professional IC Anion – MSM-HC
– MCS – LP Gradient (2.850.2230)
The 850 Professional IC Anion – MSM-HC – MCS – LP
Gradient is an intelligent ion chromatography system
for the determination of anions using high-capacity
sequential suppression and low-pressure gradient. It
may be combined with different detector types.
850 Professional IC Cation – Gradient
(2.850.1220)
The 850 Professional IC Cation – Gradient is an intelligent ion chromatography system for high pressure
gradients without suppression. This instrument may be
combined with any separation and detection method
requiring no suppression. It may be combined with different detector types.
850 Professional IC Anion – MSM-HC
– Gradient (2.850.2260)
The 850 Professional IC Anion – MSM-HC – Gradient
is an intelligent ion chromatography system for the
determination of anions with high-capacity chemical
suppression and binary high-pressure gradient. It may
be combined with different detector types.
50 — IC
Professional IC Instruments
850 Professional IC Anion – MCS
– Gradient (2.850.2220)
The 850 Professional IC Anion – MCS – Gradient is an
intelligent ion chromatography system for the determination of anions with sequential suppression and
binary high-pressure gradient. It may be combined with
different detector types.
850 Professional IC Anion – MSM-HC
– MCS – Gradient (2.850.2240)
The 850 Professional IC Anion – MSM-HC – MCS –
Gradient is an intelligent ion chromatography system
for the determination of anions with high-capacity
sequential suppression and binary high-pressure gradient. It may be combined with different detector types.
850 Professional IC instruments for anion
and cation determination
850 Professional IC AnCat – non-suppressed (2.850.3000)
The 850 Professional IC AnCat – non-suppressed is an
intelligent ion chromatography system for the determination of anions and cations without suppression. It
may be combined with different detector types.
850 Professional IC AnCat (2.850.3010)
The 850 Professional IC AnCat is an intelligent ion
chromatography system for the determination of cations without suppression and anions either with or
without chemical suppression, as required. It may be
combined with different detector types.
51 — IC
Professional IC Instruments
850 Professional IC
AnCat – MCS
(2.850.3030)
The 850 Professional IC AnCat – MCS is an intelligent
ion chromatography system for the determination of
cations without suppression and anions either with or
without sequential suppression, as required. It may be
combined with different detector types.
850 Professional IC
AnCat – MSM-HC – MCS
(2.850.3040)
The 850 Professional IC AnCat – MSM-HC – MCS is an
intelligent ion chromatography system for the determination of cations without suppression and anions
either with or without high-capacity sequential suppression, as required. It may be combined with different detector types.
52 — IC
Professional IC Instruments
Overwiew on 872 Extension Modules
2.872.0010
2.872.0030
2.872.0050
2.872.0060
2.872.0110
2.872.0120
Extension Module
IC Pump
Extension Module
IC Module
Extension Module
Sample Prep
Extension Module
Liquid Handling
Extension Module
Suppression
Extension Module
Suppression MCS
Sample Preparation
Prep 1
Prep 2
Prep 3
PP +
PP +
PP
Valve
SPM
Gradient
HPG
LPG
LPiPump
Device
iPump +
Valve
MSM
PP +
MSM
Suppression
MSM-HC
PP +
MSM-HC
yes
yes
yes
yes
yes
yes
yes
IC
Module
MCS
MCS
Liquid
Handling
PP + Valve +
Selection Valve
53 — IC
Professional IC Instruments
872 Professional IC Extension Modules
872 Extension Module IC Pump
(2.872.0010)
The 872 Extension Module IC Pump is an extension
tool for upgrading any 850 Professional IC instrument.
It allows an additional IC high-pressure pump «iPump»
to be installed in any 850 Professional IC system.
872 Extension Module IC Module
(2.872.0030)
The 872 Extension Module IC Module is an extension
tool for upgrading any 850 Professional IC instrument.
It allows an IC high-pressure pump «iPump» and an
injection valve to be installed in any 850 Professional IC
system.
872 Extension Module Sample Prep
(2.872.0050)
The 872 Extension Module Sample Prep is an extension
tool for upgrading any 850 Professional IC instrument.
It enables an additional peristaltic pump and injection
valve to be installed in any 850 Professional IC system.
872 Extension Module Liquid Handling
(2.872.0060)
The 872 Extension Module Liquid Handling is an extension tool for upgrading any 850 Professional IC instrument. It enables an additional peristaltic pump, an
additional injection valve as well as a 10-port selector
valve to be installed in any 850 Professional IC system.
54 — IC
Professional IC Instruments
872 Extension Module Suppression
(2.872.0110)
The 872 Extension Module Suppression is an extension
tool for upgrading any 850 Professional IC instrument.
It allows to install a complete chemical suppression in
any 850 Professional IC system.
872 Extension Module Suppression – MCS
(2.872.0120)
The 872 Extension Module Suppression – MCS is an extension tool for upgrading any 850 Professional IC instrument.
It allows a complete sequential suppression to be installed
in any 850 Professional IC system.
55 — IC
Compact IC Instruments
56 — IC
Compact IC Instruments
Compact IC Instruments
Compact IC – Instruments – Introduction
Compact intelligence for ion chromatography
881 Compact IC pro – 882 Compact IC plus and
883 Basic IC plus
Intelligent. Safe. Precise.
Metrohm's high-end ion chromatograph is the 850
Professional IC, whose intelligent system components
define the standards regarding precision of results
and ease of operation. This technology is now available for the Compact IC instruments as well. The 881
Compact IC pro and the 882 Compact IC plus are the
ideal choice for users from all fields of application with
clearly defined analytical requirements. These instruments ensure the rapid and safe determination of
anions, cations and polar substances in the g/L to the
g/L range.
do not include these modules. The detection mode can
be choosen. Therefore no detector is included in the
scope of delivery of the Compact IC instruments.
The 883 Basic IC plus is the ideal instrument for training in higher education. It may be used with the
included 850 Professional Conductivity Detector and
the MagIC Net™ Basic software.
All intelligent functions of the Professional IC instrument series have been integrated into the 881, 882
and 883 Compact instruments: iPump, iDetector,
iColumn technology. They guarantee precise results
and help prevent operator errors. The MagIC Net™
chromatography software controls all system components and monitors all parameters that are relevant to
the chromatographic analysis.
The 881 Compact IC pro instruments are equipped
with column heater and eluent degasser; the version
with sequential suppression comes with an additional
sample degasser. The 882 Compact IC plus instruments
57 — IC
Compact IC Instruments
Overwiew on Compact IC Instruments
Comparison on the 872 Extension Moduls
2.881.0010
MSM
MCS
Columnheater
Eluent
degasser
Sample
degasser
Automation
capability
815
included
Software
included
yes
yes
yes
2.881.0020
yes
yes
yes
yes
2.881.0030
yes
yes
yes
yes
yes
yes
2.882.0010
yes
2.882.0020
yes
yes
2.882.0030
yes
yes
yes
2.883.0020
yes
yes
yes
2.883.1020
yes
yes
yes
yes
58 — IC
Compact IC Instruments
Compact IC pro instruments
881 Compact IC pro – Cation
(2.881.0010)
The 881 Compact IC pro – Cation is an intelligent ion
chromatograph in compact design with column heating for the determination of anions, cations or polar
substances without suppression. It may be combined
with different detector types.
881 Compact IC pro – Anion
(2.881.0020)
The 881 Compact IC pro – Anion is an intelligent ion
chromatograph in compact design with column heating for the determination of anions or polar substances
with chemical suppression. It may be combined with
different detector types.
881 Compact IC pro – Anion – MCS
(2.881.0030)
The 881 Compact IC pro – Anion – MCS is an intelligent ion chromatograph in compact design with
column heating for the determination of anions or
polar substances with sequential suppression. It may be
combined with different detector types.
59 — IC
Compact IC Instruments
Compact IC plus instruments
882 Compact IC plus – Cation
(2.882.0010)
The 882 Compact IC plus – Cation is an intelligent ion
chromatograph in compact design without column
heating for the determination of anions, cations or
polar substances without chemical suppression. It may
be combined with different detector types.
882 Compact IC plus – Anion
(2.882.0020)
The 882 Compact IC plus – Anion is an intelligent ion
chromatograph in compact design without column
heating for the determination of anions or polar substances with chemical suppression. It may be combined
with different detector types.
882 Compact IC plus – Anion – MCS
(2.882.0030)
The 882 Compact IC plus – Anion – MCS is an intelligent ion chromatograph in compact design without
column heating for the determination of anions or
polar substances with sequential suppression. It may be
combined with different detector types.
60 — IC
Compact IC Instruments
Basic IC plus instruments
883 Basic IC plus (2.883.0020)
The 883 Basic IC plus is an intelligent, very compact
ion chromatograph for training and routine applications. For determination of cations and anions with
and without chemical suppression. Inclusive MagIC
Net™ Basic software and text book.
883 Basic IC plus Package (2.883.1020)
Package for the automated analysis with the 883 Basic
IC plus. For training and routine analysis. For determination of cations and anions with or without chemical
suppression. Including 883 Basic IC plus, 863 Compact
IC Autosampler, MagIC Net™ Basic software and textbook.
61 — IC
Additional IC Componets
62 — IC
Additional IC Componets
Alternative IC Components
Alternative IC Components – Introduction
Ion Chromatography is established in the laboratoies
as a powerful and flexible analysis tool. Alternative IC
components enhance the spectrum of analytes that
can be detected. They also improve sensitivity and
selectivity.
Heatable modules are applied in post-column reaction
systems as well as in Metrohm Inline Sample Preparation (MISP). Data converters export or import the chromatographic data to external integration systems and
from external detectors respectively. Electrochemical
detectors are used in stand-alone systems or in combination with conductivity detection.
63 — IC
Additional IC Componets
Heatable Reactors and Column Compartments
886 Professional Reactor (2.886.0110)
The 886 Professional Reactor is a heated module specially designed for pre-column and post-column reaction applications. It excels by its ruggedness, the high
heating speed and the possibility to run reactions up to
120 °C.
886 Professional Thermostat
(2.886.0210)
The 886 Professional Thermostat is a stand-alone Column oven for up to two columns with a maximum
length of 150 mm. It excels by its ruggedness, the high
heating speed and the possibility to run reactions up to
80 °C.
IC interfaces
891 Professional Analog Out
(2.891.0010)
The 891 Professional Analog Out is an additional module
for intelligent IC instruments. It allows to transfer analog
signals of different chromatographic data to external
data systems.
64 — IC
Additional IC Componets
771 IC Compact Interface (2.771.0010)
Universal analog-digital converter with two channels
and 24-bit resolution. Data is transferred to the PC
via an RS 232C interface for processing by IC Net or
MagIC Net™ software.
771 IC Compact Interface; MagIC Net™
Professional (2.771.0110)
IC Compact Interface with MagIC Net™ Professional
software. The 771 Compact Interface connects the
analog signals of the existing IC instruments (Compact,
Modular and Advanced) with the improved capabilities
of the client/server and database-based technology of
the MagIC Net™ software.
771 IC Compact Interface; MagIC Net™
Compact (2.771.0210)
IC Compact Interface with MagIC Net™ Compact Software. The 771 Compact Interface connects the analogue signals of the existing IC instruments (Compact,
Modular and Advanced) to the improved capabilities of
the client/server and database-based technology of the
MagIC Net™ software.
65 — IC
Additional IC Componets
Electrochemical detectors
791 VA Detector (2.791.0020)
Amperometric Detector for Ion Chromatography.
Electrochemical (amperometric) detection with the 791
VA Detector is a very sensitive detection method used
successfully in both HPLC and ion chromatography.
This method is also characterized by its very high selectivity: Only easily oxidizable or reducible substances are
detected – chloride or sulfate are not detected and do
not interfere with the electrochemical determination,
even in high concentrations.
The detector can be used in series or in parallel with
other detectors that are frequently used in IC or HPLC
(e.g. conductivity or UV/VIS detectors).
Numerous electrodes suitable for each amperometric
application are available.
871 Advanced Bioscan (2.871.0010)
Pulsed amperometric detector for the highly sensitive
determination of sugars, sugar alcohols and sugar
acids, polysaccharides and other oxidizable substances.
The 871 Advanced Bioscan extends the IC program
from Metrohm by adding carbohydrate analysis to the
capabilities of ion chromatography. The heart of the
871 Advanced Bioscan is the pulsed amperometric
detector with built-in injector and column heater. The
system is controlled by the Metrodata IC Net software.
Besides carbohydrates the 871 Advanced Bioscan is
used to determine oxidizable inorganic anions. There
are different measuring cells with either gold, silver,
platinum or glassy carbon as electrode material available.
66 — IC
Professional IC – Hyphenated Technologies
Professional IC – Hyphenated systems
IC – Hyphenation
The capabilities of ion chromatography is expanded
considerably when Metrohm IC is coupled with other
analytical methods, sample preparation techniques or
detection systems.
The possibilities are practically unlimited. Any system
which can process aqueous solutions as samples
or which provides the same can be coupled with
Metrohm IC instruments.
Thus, for example, ion chromotography can be combined with Metrohm titrators and measuring instruments as hyphenated systems. These TitrIC systems
enable users to determine the complete range of relevant parameters in water analysis from a single sample.
Additional typical examples are the coupling of the IC
with MS or ICP-MS, Combustion IC and air monitoring
systems.
67 — IC
Professional IC – Hyphenated Technologies
Professional IC Hyphenated systems
TitrIC 4 hyphenated IC and titration
system (TitrIC 4)
TitrIC 4 – the Basic System
Fully automatic system for the direct measuring of
temperature, conductivity and pH; the titrimetric determination of p-value, m-value, calcium and magnesium;
and the determination of anions by ion chromatography.
The system consists of the 856 Conductivity Module,
four 800 Dosino dosing systems, 802 Stirrer (rod stirrer), 905 Titrando, 815 Robotic USB Sample Processor
XL and 881 Compact IC pro with sequential suppression and the 850 Professional Conductivity Detector
«iDetector».
TitrIC – the power pack for ion analysis.
TitrIC 5 hyphenated IC and titration
system (TitrIC 5)
TitrIC 5 – for the complete analysis of anions
and cations.
Fully automatic system for the direct measurement of
temperature, conductivity and pH, the titrimetric determination of the p-value and m-value; and the determination by ion chromatography of cations (including
calcium and magnesium) and anions.
The system consists of the 856 Conductivity Module,
three 800 Dosino dosing systems, 802 Stirrer (rod stirrer), 855 Robotic Titrosampler, one 881 Compact IC
pro without suppression and one 881 Compact IC pro
with sequential suppression with one 850 Professional
Conductivity Detector «iDetector» each.
TitrIC – the power pack for ion analysis.
68 — IC
Professional IC – Hyphenated Technologies
TitrIC 6 hyphenated IC and titration
system (Titric 6)
TitrIC 6 – the professional solution with sealed
sample vessels.
Fully automatic system for the direct measurement of
temperature, conductivity and pH; the titrimetric determination of the p-value and m-value; and the determination by ion chromatography of cations (including
calcium and magnesium) and anions. The sample
changer is equipped with the DisCover function for
automatically removing the sample vessel covers.
The system consists of the 856 Conductivity Module,
three 800 Dosino dosing systems, 802 Stirrer (rod stirrer), one 905 Titrando, one 815 Robotic USB Sample
Processor XL and one 850 Professional IC with two
850 Professional Conductivity Detectors «iDetectors»
for anions (sequential suppression) and cations.
TitrIC – the power pack for ion analysis.
TitrIC 7 hyphenated IC and titration
system (TitrIC 7)
TitrIC 7 – the solution for samples containing
particles.
Fully automatic system for the direct measurement of
temperature, conductivity and pH; the titrimetric determination of the p-value and m-value; and the determination by ion chromatography of cations (including
calcium and magnesium) and anions. Particle-containing samples have their particles removed by Metrohm
Inline Ultrafiltration prior to determination by ion chromatography.
The system consists of the 856 Conductivity Module,
two 800 Dosino dosing systems, one 802 Stirrer (rod
stirrer), one 855 Robotic Titrosampler, one 850 Professional IC – Anion – Prep 2 with one 850 Professional
Conductivity Detector «iDetector» for anions and one
872 Extension Module IC Pump with an additional iDetector for cation analysis.
TitrIC – the power pack for ion analysis.
IC-MS and IC-ICP/MS Coupling
Combining IC with an electrospray ionization mass
spectrometer (ESI-MS) or an inductively coupled plasma
mass spectrometer (ICP-MS) solves even complex
separation problems while achieving outstanding sensitivities and selectivities. These so-called hyphenated
techniques provide valuable information for unambiguous peak identification and are less prone to matrix
influences than IC with conductivity detection.
69 — IC
Professional IC – Hyphenated Technologies
Combustion IC (Mitsubishi) (CIC)
The Mitsubishi Automatic Quick Furnace AQF-100 – a
combustion preparation station – is easily combined
with Metrohm ion chromatography equipment. This
results in a fully automated combustion system. This
opens up a completely new range of samples, from viscous to solid, for fast and accurate elemental analysis.
MultiTek Combustion IC (230 V)
(2.881.2034)
The complete Combustion IC system. The 881 Compact IC pro is combined with the MultiTek Horizontal
IC manufactured by PAC. This results in a fully automated combustion system. This opens up a completely
new range of samples, from viscous to solid, for fast
and accurate elemental analysis.
MultiTek Combustion IC (110 V)
(2.881.2035)
The complete Combustion IC system. The 881 Compact IC pro is combined with the MultiTek Horizontal
IC manufactured by PAC. This results in a fully automated combustion system. This opens up a completely
new range of samples, from viscous to solid, for fast
and accurate elemental analysis.
PILS, Particle Into Liquid Sampler
(2.136.0400)
Particle into Liquid Sampler for the collection of ambient aerosols. Coupling with ion chromatographs allows
automatic determination of the ionic composition of
the aerosols without requiring additional sample preparation.
70 — IC
Professional IC – Hyphenated Technologies
MARGA, Monitor for Aerosols and
Gases in Air (MARGA)
MARGA is a fully automated online system for the
determination of anions and cations in gases and
aerosols. The acidic and alkaline gasses are absorbed
in water in a «Wet Rotating Denuder» and the aerosols
in a «Steam Jet Aerosol Collector» and then analyzed
for anion and cation content with two Compact ICs.
MARGA is intended for unattended use over a longer
period.
MARGA is available from Applikon www.applikon.com.
71 — IC
Automation in Ion Chromatography
72 — IC
Automation in Ion Chromatography
IC Automation
IC Automation – Introduction
Sample changer
Automation in ion chromatography ranges from
straight-forward sample intorduction to highly sophisticated combined sample preparation. Sample volumes
from a few L up to several mL need to be handled. A
number of sample changers for the different application fields are available.
tion, Dialysis, Preconcentration, Matrix Elimination,
Matrix Neutralisation and Inline Calibration.
IC Equipment for liquid handling
MISP made easy: The IC equipment sets contain all the
necessary modules for the relevant sample preparation
method. This means that you can be certain that the
method will work properly.
The 858 Professional Sample Processor is more than
just a sample changer. Equipped with pumps, highpressure valve and Dosino dosing systems, it greatly
enhances capabilities in inline sample preparation and
liquid handling.
In addition to the 858 Professional Sample Processor,
the 889 IC Sample Center, and the 863 Compact IC
Sample the 814 and 815 Sample Processors are available from the titration product line.
Metrohm inline sample preparation
(MISP)
Samples such as milk, chocolate, soda lye, biodiesel or
strongly polluted wastewater require sample preparation before they can be analysed by IC. The 850 Professional IC together with the 858 Professional Sample
Processor offers numerous possibilities for completely
automating Inline Sample Preparation, e.g. Ultrafiltra-
73 — IC
Automation in Ion Chromatography
Overwiew on IC Automation
858
863
889
814
815
Variable: 999
11 mL Vials: 148
Fixed rack,
with 36 positions
Variable: 384
0,7 mL Vials: 96
Variable: 999
11 mL Vials: 148
Variable: 999
11 mL Vials: 228
External position
yes
no
no
yes
yes
Sample delivery
Dual channel
peristaltic pump
or 800 Dosino
Dual channel
peristaltic pump
or 800 Dosino
Microliter syringe
800 Dosino
800 Dosino
yes, as Option
no
yes
no
no
Positions on sample rack
Injection valve
MSB
3x
no
no
3x
3x
Sample volume
0.5 500 mL
0.5 11 mL
0.001 10 mL
0.5 500 mL
0.5 500 mL
«MISP»
All techniques
Limited selection
Limited selection
Some techniques
Some techniques
74 — IC
Automation in Ion Chromatography
IC automation – instruments
858 Professional Sample Processor
(2.858.0010)
The 858 Professional Sample Processor processes
samples with volumes ranging from 500 L to 500 mL.
Sample transfer is carried out either by using the peristaltic pump of the 850 Professional IC system or by an
800 Dosino.
858 Professional Sample Processor
– Pump (2.858.0020)
The 858 Professional Sample Processor – Pump processes samples with volumes ranging from 500 L to
500 mL. Sample transfer is carried out either by using
the built-in bidirectional dual-channel peristaltic pump
or by an 800 Dosino.
858 Professional Sample Processor
– Pump – Injector (2.858.0030)
The 858 Professional Sample Processor – Pump – Injector processes samples with volumes ranging from 500
L to 500 mL. Sample transfer is carried out either by
using the built-in bidirectional dual-channel peristaltic
pump or by an 800 Dosino. Additionally a six-port
injection valve is available for sample preparation purposes.
889 IC Sample Center (2.889.0010)
The 889 IC Sample Center is a robust autosampler for
high sample throughput. Optimized for the challenges
of modern analytical labs, the 889 IC Sample Center
uses the x-y-z principle and a high-resolution dosing for
sample introduction. A double needle system allows
the use of vials with caps or septa. A PEEK-injector
completes the automation of the 889 IC Sample Center. The 889 IC Sample Center is the perfect automation tool when only very little sample is available.
75 — IC
Automation in Ion Chromatography
889 IC Sample Center – cool
(2.889.0020)
The 889 IC Sample Center is the perfect automation
tool if only very little sample is available. Additional to
the 889 IC Sample Center it is equipped with a cooling
function and is therefore the perfect autosampler for
biochemical and/or thermally instable samples.
815 Robotic Soliprep for LC
(2.815.4110)
The 815 Robotic Soliprep for Liquid Chromatography is
a complete system for the fully automated preparation
of samples that have to be dissolved, homogenized,
diluted or filtered prior to analysis. The system includes
the following instruments:
1
1
1
2
2
x
x
x
x
x
815
136
772
786
800
Robotic USB Sample Processor XL
Polytron with power supply
Pump Unit
Swing Head
Dosino
863 Compact IC Autosampler
(2.863.0010)
The 863 Compact IC Autosampler is the ideal automation solution for routine analysis. Using the 863 Compact IC Autosampler all Metrohm ion chromatographs
can be automated.
76 — IC
Automation in Ion Chromatography
Additional Sample Processors for the IC
Even more choice and flexibility!
MagIC Net™ allows users to run USB Sample Processors from our titration portfolio. This translates into
virtually unlimited capabilities in automating your
ion chromatographic analyses. Whether small or big
sample beakers, whether at room temperature or
under cooling conditions, whether you use a sample
processor with one or two towers, our answer to your
demands in ion chromatography always is:
Yes, we can!
The benefits of using a sample processor are not limited to saving time: Automated systems control repetitive operation steps improving both reproducibility
and accuracy. Errors can be almost completely eliminated. Day or night, your sample series are processed
with maximum precision. Whether automated sample
preparation, liquid handling or sample analysis – this
new generation of sample processors features capabilities hitherto available only in robots.
Apart from MagIC Net™ and depending on your
preferences the USB Sample Processor can also be controlled by Touch Control, PC Control or by our titration software tiamo™.
Ordering information
2.814.0010 814 USB Sample Processor (1T/1P)
2.814.0020 814 USB Sample Processor (1T/2P)
2.814.0030 814 USB Sample Processor (1T/0P)
2.814.0110 814 USB Sample Processor (2T/2P)
2.814.0120 814 USB Sample Processor (2T/4P)
2.814.0130 814 USB Sample Processor (2T/0P)
2.815.0010 815 Robotic USB Sample Processor XL
(1T/1P)
2.815.0020 815 Robotic USB Sample Processor XL
(1T/2P)
2.815.0030 815 Robotic USB Sample Processor XL
(1T/0P)
2.815.0110 815 Robotic USB Sample Processor XL
(2T/2P)
2.815.0120 815 Robotic USB Sample Processor XL
(2T/4P)
2.815.0130 815 Robotic USB Sample Processor XL
(2T/0P)
2.815.2110 815 Robotic Flexible Soliprep
2.815.3110 815 Robotic Filtration Soliprep
2.136.0654 MultiTek Autosampler 10 L (230 V)
2.136.0655 MultiTek Autosampler 10 L (110 V)
2.136.0664 MultiTek Autosampler 25 L (230 V)
2.136.0665 MultiTek Autosampler 25 L (110 V)
814 USB Sample Processor with sample rack for 12 x 250 mL
77 — IC

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